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FEATURES AFFECTING THE JOINING PROCESS OF CERAMIC MATERIALS

机译:影响陶瓷材料接合过程的特征

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摘要

Examples of joining techniques applied to various ceramic materials are presented and related to the principal features that must be controlled in order to realize a reliable bond. Adhesion between two ceramic materials can be obtained by exploiting their specific microstructural and compositional characteristics. In particular, the interfacial forces, that act during the sintering process and determine the final microstructure of the materials, play an important role even during bonding. The intergranular force balance change with temperature, applied pressure and in the presence of new compounds. Moreover, when a liquid phase that wets well the main ceramic phase is involved in a bonding process, adhesion can be promoted by the capillary force that arises at the meniscus between two surfaces in contact. The consequent interaction between the ceramic grains at the interface and the liquid phase determines the final microstructure and properties of the joint. Results are presented for oxide (AL_2O_3, ZrO_2 and AL_2O_3/ZrO_2 composite) and non oxide (Si_3N_4 and SiC) dense ceramics, bonded with a metal or a glass interlayer or with no interlayer, with or without an applied pressure. The chemical stability and the mutual mobility of the phases involved are investigated. The microstructure of the interfacial region is analysed and related to the flexural strength values and other mechanical and compositional features of the materials.
机译:介绍了应用于各种陶瓷材料的连接技术的示例,这些示例与必须控制以实现可靠结合的主要特征有关。两种陶瓷材料之间的粘附力可以通过利用其特定的微观结构和组成特性来获得。尤其是在烧结过程中起作用并确定材料最终微观结构的界面力,即使在粘结过程中也起着重要的作用。晶间力平衡随温度,施加的压力以及存在新化合物而变化。此外,当在粘结过程中涉及润湿主要陶瓷相的液相时,可以通过在接触的两个表面之间的弯液面处产生的毛细作用力来促进粘附。界面处的陶瓷颗粒与液相之间的相互作用决定了接头的最终微观结构和性能。给出了在有或没有施加压力的情况下,与金属或玻璃夹层或无夹层结合的氧化物(AL_2O_3,ZrO_2和AL_2O_3 / ZrO_2复合材料)和非氧化物(Si_3N_4和SiC)致密陶瓷的结果。研究了所涉及各相的化学稳定性和相互迁移性。分析了界面区域的微观结构,并将其与材料的抗弯强度值以及其他机械和组成特征相关联。

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