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3D atom probe investigation of nanocomposite wires

机译:纳米复合线材的3D原子探针研究

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摘要

Two kinds of high strength nanocomposite wires produced under heavy plastic deformation were investigated using 3D Atom Probe. First, cold drawn pearlitic steel wires were analysed. Partly dissolved cementite lamellae were mapped out in 3D. The surface to volume ratio of cementite lamellae was correlated to their dissolution rate. Considering the increase of the interfacial energy during drawing, a model based on simple thermodynamical arguments was developed to estimate the global dissolution rate of cementite. Cu/Nb nanocomposite wires were also studied. Their nanoscale cross-section microstructure was revealed for the first time. 3D Atom Probe analysis pointed out a slight inter-diffusion of copper and niobium, and steps in copper channels attributed to tracks of moving dislocations in the (111) Cu plane, along the <110> direction.
机译:使用3D原子探针研究了在严重塑性变形下生产的两种高强度纳米复合金属丝。首先,对冷拔珠光体钢丝进行分析。 3D绘制了部分溶解的渗碳体薄片。渗碳体薄片的表面体积比与其溶解速率相关。考虑到拉拔过程中界面能的增加,建立了基于简单热力学论证的模型来估算渗碳体的整体溶出率。还研究了Cu / Nb纳米复合线。首次揭示了它们的纳米级横截面微观结构。 3D Atom Probe分析指出,铜和铌之间有少量相互扩散,并且铜通道中的台阶归因于沿(110)方向在(111)Cu平面中移动的位错的轨迹。

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