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Nanocrystalline TiN Coating Prepared by Reactive Plasma Spraying

机译:等离子喷涂制备纳米晶TiN涂层

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摘要

A gas-tunnel plasma spraying gun was self-designed. The titanium powders and nitrogen gas were used as the reactants to produce dense TiN coating by means of the reactive plasma spraying (RPS) technique. RPS is a promising technique that enables the fabrication of dense composite coatings with a metallic or an intermetallic matrix and finely dispersed ceramic phases. The TiN coating is of great thickness (> 500 μm) and composed of nanocrystallities. In this respect, a new nano-materials fabrication technology was developed. The nanocrystalline TiN coating was examined using XRD, TEM and HRTEM. Results show that the coating is of well-stoichiometry, which is composed of TiN crystals of about 50-70nm in diameter, as well as the amorphous TiN phase. The nanocrystallities are separated by small-angle (about 7) grain boundaries.
机译:自行设计了气体隧道等离子喷枪。钛粉和氮气用作反应物,通过反应等离子体喷涂(RPS)技术产生致密的TiN涂层。 RPS是一种有前途的技术,它能够制造具有金属或金属间化合物基质和精细分散的陶瓷相的致密复合涂层。 TiN涂层的厚度很大(> 500μm),并且由纳米晶体组成。在这方面,开发了一种新的纳米材料制造技术。使用XRD,TEM和HRTEM检查了纳米晶TiN涂层。结果表明该涂层具有良好的化学计量,它由直径约为50-70nm的TiN晶体以及非晶态的TiN相组成。纳米晶体被小角度(约7个)晶界隔开。

著录项

  • 来源
  • 会议地点 Shenyang(CN)
  • 作者单位

    Department of Materials Science and Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China;

    Department of Materials Science and Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China;

    Department of Materials Science and Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China;

    Department of Materials Science and Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China;

    Department of Materials Science and Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China;

    Department of Materials Science and Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China;

  • 会议组织
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    nanocrystalline; TiN coating; reactive plasma spray;

    机译:纳米晶TiN涂层;反应等离子喷涂;

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