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PARTIALLY ALIGNED PIEZOELECTRIC NANOFIBERS BY SOL-GEL ELECTROSPINING PROCESS

机译:溶胶凝胶电喷雾法部分校正压电纳米粒子

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摘要

This paper reports the fabrication of partially aligned Lead Zirconate Titanate (PZT) nanofibers with an average diameter of 150 nm by Sol-Gel Electrospinning process. Both randomly distributed and uniaxially aligned PZT fibers were obtained from the sol-gel PZT solution with viscosity modified by polyvinyl pyrrolidone (PVP). The diameters of the nano fibers can be further reduced or controlled for different applications. SEM, TEM and x-ray diffraction (XRD) are used to characterize the nano-fibers and their crystal structures. XRD confirmed that pure perovskite phase was formed after the as-spun fibers being annealed at about 650℃. Different approaches have been explored to fabricate the uniaxially-aligned PZT nano-fibers. Microelectromechanical (MEMS) based micro-fabrication technologies are used to assist the development of the nano-fibers in designing the test samples, depositing and patterning the electrodes, and also testing the performance of the nano fibers.
机译:本文报道了通过Sol-Gel电纺丝工艺制备的平均直径为150 nm的部分排列的钛酸锆钛酸铅(PZT)纳米纤维。从具有聚乙烯吡咯烷酮(PVP)改性的粘度的溶胶-凝胶PZT溶液中获得随机分布和单轴排列的PZT纤维。可以进一步减小或控制纳米纤维的直径以用于不同的应用。 SEM,TEM和X射线衍射(XRD)用于表征纳米纤维及其晶体结构。 XRD证实初生纤维在约650℃退火后形成纯钙钛矿相。已探索出不同的方法来制造单轴排列的PZT纳米纤维。基于微机电(MEMS)的微细加工技术可用于协助纳米纤维的开发,包括设计测试样品,沉积和构图电极以及测试纳米纤维的性能。

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