Preparation and Characterization of TiO_2 Film on Glass Flake

机译：玻璃鳞片上TiO_2薄膜的制备与表征

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A TiO_2 film was prepared on glass flake with Ti(OBu)_4 as a main material by peptization and reflux method at 80℃ in acidic abundant aqueous solution. The surface topography and surface phase structure were characterized by scanning electron microscope, energy spectrum, X-ray diffractometer, X-ray photoelectron spectroscope, and the bonding strength between film and glass flake was researched by ultrasonic vibration. The results indicated that the TiO_2 film, the main phase was anatase and a little rutile, coated on the glass flake uniformly. Along with growth of TiO_2 on surface of glass flake, the formation maybe base on two different mechanics, at the earlier stage, TiO_2 coupled surface of glass flake with Si-O-Ti chemical bond, but with physical deposition at final.

机译：以Ti（OBu）_4为主要原料，在80℃酸性富水溶液中通过胶溶和回流法在玻璃鳞片上制备了TiO_2薄膜。通过扫描电子显微镜，能谱，X射线衍射仪，X射线光电子能谱对表面形貌和表面相结构进行表征，并通过超声振动研究薄膜与玻璃鳞片之间的结合强度。结果表明，TiO_2薄膜的主要相为锐钛矿型，略带金红石型，均匀地涂覆在玻璃鳞片上。随着TiO_2在玻璃鳞片表面的生长，其形成可能是基于两种不同的机理，在较早阶段，TiO_2耦合了具有Si-O-Ti化学键的玻璃鳞片表面，但最终发生了物理沉积。

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来源
《Inorganic thin films and coatings》|2012年|220-223|共4页
会议地点 Guilin(CN)
作者
Yi Guo; Shiguo Du; Jun Yan; Bin Wang;
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作者单位

Shijiazhuang Mechanical Engineering College, Shijiazhuang, Hebei province, P.R.China;

Shijiazhuang Mechanical Engineering College, Shijiazhuang, Hebei province, P.R.China;

Shijiazhuang Mechanical Engineering College, Shijiazhuang, Hebei province, P.R.China;

Shijiazhuang Mechanical Engineering College, Shijiazhuang, Hebei province, P.R.China;

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会议组织
原文格式 PDF
正文语种 eng
中图分类
关键词
Glass flake; TiO_2; Film;

机译：玻璃鳞片; TiO_2;电影;

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Preparation and Characterization of TiO_2 Film on Glass Flake

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