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Control of Reactive Deposition Process by Stabilization of the Power Supply Work

机译:通过稳定电源工作来控制无功沉积过程

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Oxide coatings deposition in reactive process from metallic targets has particular importance thanks to cheapness of metallic target in comparison with conductive ceramic targets. Silicon oxide can be deposited only from a metallic target or from dielectric target by RF-sputtering, but deposition speed in case of RF-sputtering is low. Reactive sputtering of metallic targets is characterized by voltage hysteresis and has a characteristic appearance depending on type of metal and value of secondary electronic emission factor for metal and oxide. From voltage-current (VC) characteristics follows, that for silicon oxide (SiO_2) deposition it is necessary to work in power supply constant voltage mode and for titanium oxide (TiO_2) deposition - at constant current mode and at constant oxygen flow. For process stabilization it is necessary to stabilize the second electric parameter by changing oxygen flow in the chamber. We develop an algorithm and a control system of process for this case. As a result in process there is only one variable value of process which can be controlled, this is oxygen flow, at a constant pumping speed, leakage, etc. In this case process will be stabilized. Changes of outgasing flow during process as a result of heating of design elements of a chamber will be considered also. Stabilization of parameters of the power supply creates favorable conditions for repro-ducibility of properties of a coating. In the work results of process stabilization are presented at SiO_2 and TiO_2 coating deposition on polymeric PET film.
机译:由于金属靶材与导电陶瓷靶材相比便宜,因此在反应过程中从金属靶材沉积氧化物涂层尤为重要。只能通过射频溅射从金属靶或介电靶上沉积氧化硅,但是在射频溅射的情况下沉积速度很低。金属靶材的反应溅射具有电压滞后特性,其外观取决于金属的类型以及金属和氧化物的二次电子发射因子的值。从电压-电流(VC)特性可以得出,对于氧化硅(SiO_2)沉积,必须在电源恒定电压模式下工作,对于氧化钛(TiO_2)沉积-必须在恒定电流模式下和恒定氧气流量下工作。为了过程稳定,必须通过改变腔室中的氧气流量来稳定第二电参数。我们针对这种情况开发了一种算法和过程控制系统。作为过程的结果,只能控制一个可变的过程值,这是氧气流量,恒定的泵速,泄漏等。在这种情况下,过程将稳定。还应考虑由于加热腔室的设计元素而导致的处理过程中排气流量的变化。电源参数的稳定为涂层性能的可再现性创造了有利的条件。在工作中,在聚合物PET薄膜上的SiO_2和TiO_2涂层沉积过程中,获得了过程稳定化的结果。

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