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Mechanical properties of SiOx coated PET films characterized by AFM equipped with micro tensile stage

机译:配备微拉伸台的AFM表征SiOx涂覆的PET膜的机械性能

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Direct observation of early stage fragmentation of nanosized SiO_x coating deposited by PECVD onpoly(ethylene terephthalate) (PET) film substrates is investigated by means of micro tensile device coupled with atomic force microscope (AFM). This arrangement allows fast measurement of fragmentation patterns of SiOx coatings with thickness below 30 nm. Nanometer thick SiO_x coatings are deposited on three grades of PET films containing predetermined anti-blocking particle density ranging from 0 to 1800 mm~(-2). Crack onset strain and fragment densities of SiO_x coatings are compared with previously obtained data from SEM observations. The results confirm the negative influence of anti-blocking particles on mechanical properties of coatings. The cohesion strength and the interfacial adhesion are modeled using a constant interfacial strength approach with a Weibull-type probability of fracture.
机译:通过结合原子力显微镜(AFM)的微拉伸装置研究了通过PECVD在聚对苯二甲酸乙二醇酯(PET)薄膜基材上沉积的纳米SiO_x涂层的早期碎裂的直接观察。这种布置可以快速测量厚度小于30 nm的SiOx涂层的碎裂图案。将纳米级的SiO_x涂层沉积在三种级别的PET薄膜上,这些薄膜的预定防粘连颗粒密度范围为0至1800 mm〜(-2)。将SiO_x涂层的裂纹起始应变和碎片密度与先前从SEM观测中获得的数据进行比较。结果证实了抗粘连颗粒对涂层机械性能的负面影响。使用具有Weibull型断裂概率的恒定界面强度方法对内聚强度和界面粘合性进行建模。

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