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Study on the thermal stability of aluminum nanostructure

机译:铝纳米结构的热稳定性研究

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Al nano-particles were prepared by a dry roller vibration milling at room temperature, and the particles size milled 4 hour was the range between 50 and 80nm. The products were annealed 2 hour in the extent of 100°C–330°C. By XRD and DSC testing, we study the effect heat treatment temperature on Al particles size and microstructure. The research indicated that Al nano-particles located in metastable high energy state, because the partial mechanical energy intake the material interior in the process of vibration milling with distortion and fault. Through some heat disorder, the surface energy, strain energy and fault energy of the material can mutually conversion.In the range from 240°C to 300°C, the deposited energy was given out resulting in the material interior energy reducing.
机译:通过在室温下进行干辊振动研磨来制备Al纳米颗粒,并且研磨4小时的粒径为50至80nm。产品在100°C–330°C的温度下退火2小时。通过XRD和DSC测试,我们研究了热处理温度对Al颗粒尺寸和微观结构的影响。研究表明,Al纳米粒子处于亚稳态的高能态,这是因为部分机械能在振动铣削过程中以变形和断层的形式吸收了材料的内部。通过一些热失调,材料的表面能,应变能和断裂能可以相互转换。在240°C至300°C的范围内,沉积的能量被释放出来,从而导致材料内部的能量减少。

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