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Preparation and magnetic properties of silane modified Ni-Zn ferrite and its epoxy composites

机译:硅烷改性镍锌铁氧体及其环氧复合材料的制备及磁性

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Ni-Zn ferrite/epoxy composites were investigated for embedded inductors. Ni-Zn ferrite power was prepared by a chemical coprecipitation method, and then modified with γ-glycidoxypropyl trimethoxysilane (KH-560). The unmodified ferrite was characterized by a powder X-ray diffraction (XRD) and vibrating sample magnetometer (VSM). The XRD curve showed that the ferrite was typical spinel structure, and the measuring result of the VSM indicated that the initial permeability of the ferrite was about 1225.03. The magnetic epoxy composites were respectively fabricated by mixing the modified or unmodified ferrite and epoxy resin. The composites made from the modified-ferrite exhibited better dispersion than that from the unmodified. Magnetic properties of composites were measured by Agilent E 4991 A. The results showed that the permeability of the epoxy composite was rising from 1.4 to 2.1 with the mass fraction of the ferrite increasing in the composite from 30% ∼ 70%, and magnetic loss was low.
机译:研究了用于嵌入式电感器的Ni-Zn铁氧体/环氧树脂复合材料。通过化学共沉淀法制备Ni-Zn铁氧体电源,然后用γ-环氧丙氧基丙基三甲氧基硅烷(KH-560)进行改性。未改性的铁氧体通过粉末X射线衍射(XRD)和振动样品磁强计(VSM)进行表征。 XRD曲线表明,铁素体是典型的尖晶石结构,VSM的测量结果表明,铁素体的初始磁导率约为1225.03。通过混合改性或未改性的铁氧体和环氧树脂分别制备磁性环氧复合材料。由改性铁氧体制成的复合材料表现出比未改性铁氧体更好的分散性。用Agilent E 4991 A测量了复合材料的磁性能。结果表明,随着复合材料中铁素体的质量分数从30%到70%的增加,环氧复合材料的磁导率从1.4升高到2.1。低的。

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