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HRTEM Study of Precipitates at the Early Stage during Aging in Al-Mg-Si-Cu Alloy

机译:在Al-Mg-Si-Cu合金中老化期间早期沉淀物的HRTEM研究

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The effect of copper on precipitation sequence of Al-Mg-SI alloys has been studied and discussed by many researchers. However, there is no suitable explanation yet. We are studying precipitation sequence of Al-Mg-Si alloys by using high-resolution transmission electron microscopic (HRTEM) technique. Several metastable phases and their crystal structures as well as the lattice parameter have been determined by our previous research. We have found the segregation of copper happening at the interface between the Q'-phase in the Al-Mg-Si-Cu alloy by energy-filtering TEM (EFTEM). Also, strange shape precipitate was found at that time and we have reported about it at the 8th ICAA [1]. In this work, we observed the precipitate, which has the elongated shape in the sample annealed at the early stage during aging and discussions about its crystal lattice and the differences between this precipitate and the normal ones in this alloy, for example, Q'-,b"-,b'- phases were presented.
机译:研究了许多研究人员研究和讨论了铜对Al-Mg-Si合金沉淀序列的影响。但是,没有合适的解释。我们通过使用高分辨率透射电子显微镜(HRTEM)技术研究Al-Mg-Si合金的沉淀序列。通过我们以前的研究确定了几个稳定性阶段及其晶体结构以及格子参数。我们发现通过能量滤波TEM(EFTEM)在Al-Mg-Si-Cu合金中Q'-相之间的界面处发生铜的分离。此外,当时发现奇怪的形状沉淀,我们已经在第8次ICAA [1]中报道了它。在这项工作中,我们观察到沉淀物,该沉淀物在老化和讨论其晶格期间在早期阶段的样品中的细长形状和该沉淀物与该合金中的正常情况之间的差异,例如Q'- B“ - ,B'-阶段呈现。

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