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A NOVEL CARBON NANOTUBES SYNTHESIS CONTINUOUS PROCESS USING IRON FLOATING CATALYST ON MGO PARTICLES FOR CVD OF METHANE IN A FLUIDIZED BED REACTOR

机译：一种新型碳纳米管合成使用铁浮催化剂在流化床反应器中甲烷CGD颗粒上的铁浮催化剂合成连续方法

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A novel continuous process was employed for synthesis of carbon nanotubes (CNTs) by catalytic chemical vapor deposition (CCVD) of methane over Fe/MgO using a combination of a fluidized bed reactor and a floating catalyst. MgO, fluidized by methane as the carbon source, was transferred to top of the hot zone of a fluidized reactor, where ferrocene vapor was introduced. Ferrocene decomposes in the reactor hot zone and iron nanoparticles deposit on the MgO. CNTs are grown by CCVD of methane on the in-situ produced Fe/MgO catalyst, on its flow along the reactor. More efficient contact of the ferrocene and MgO was obtained by placing an annular tube in the ferrocene-MgO contact region. CNTs are only grown when the MgO as the support was introduced into the reactor. Dense entangled bundles of 20-30 nm CNTs with Raman I_G/I_D of about 10, indicating high quality CNTs with low amorphous carbon impurities, were obtained when the annular contactor was used.

机译：使用流化床反应器和浮催化剂的组合，使用新的连续方法来合成甲烷的催化化学气相沉积（CCVD）通过Fe / MgO的催化化学气相沉积（CCVD）。由甲烷流化作为碳源的MgO被引入流化反应器的热区的顶部，其中介绍了二茂铁蒸气。二茂铁在MgO的反应器热区和铁纳米粒子沉积物中分解。 CNT通过甲烷的CCVD在原位生产的Fe / MgO催化剂上生长在其沿反应器的流动。通过将环形管放置在铁茂胶导体接触区域中获得更有效地接触。仅当MgO作为载体引入反应器时仅生长CNT。当使用环形接触器时，获得了约10的拉曼I_G / I_D的浓度为20-30nm cnts，约10，表示具有低无定形碳杂质的高质量CNT。

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《International Carbon Conference》|2007年||共2页
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S. Maghsoodi; Y. Mortazavi; A. Khodadadi;
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中图分类碳及其无机化合物;
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1. A novel continuous process for synthesis of carbon nanotubes using iron floating catalyst and MgO particles for CVD of methane in a fluidized bed reactor [J] . Sarah Maghsoodi, Abasali Khodadadi, Yadollah Mortazavi Applied Surface Science . 2010,第9期

机译：在流化床反应器中使用铁浮催化剂和MgO颗粒进行甲烷CVD的新型连续碳纳米管合成方法
2. Growth of single-walled carbon nanotubes on a Co—Mo—MgO supported catalyst by the CVD of methane in a fixed bed reactor: Model setting and parameter estimation [J] . Nosrat Izadi, Ali Morad Rashidi, Bahman Amini Horri Solid state sciences . 2011,第6期

机译：在固定床反应器中通过甲烷的CVD在Co-Mo-MgO负载的催化剂上单壁碳纳米管的生长：模型设置和参数估计
3. Production of single-walled carbon nanotubes from methane over Co-Mo/MgO nanocatalyst: A comparative study of fixed and fluidized bed reactors [J] . Alimorad Rashidi, Roghayeh Lotfi, Ehsaneh Fakhrmosavi, 天然气化学（英文版） . 2011,第004期

机译：在Co-Mo / MgO纳米催化剂上由甲烷生产单壁碳纳米管：固定床和流化床反应器的比较研究
4. A NOVEL CARBON NANOTUBES SYNTHESIS CONTINUOUS PROCESS USING IRON FLOATING CATALYST ON MGO PARTICLES FOR CVD OF METHANE IN A FLUIDIZED BED REACTOR [C] . S. Maghsoodi, Y. Mortazavi, A. Khodadadi International Carbon Conference(Carbon 2007); 20070715-20; Seattle,WA(US) . 2007

机译：在流化床反应器中用MGO颗粒上的铁浮选催化剂进行甲烷合成的新型碳纳米管连续过程
5. Synthesis of carbon nanotubes by microwave plasma enhanced CVD on silicon using iron as catalyst. [D] . Nidadavolu, Anandha G. R. 2005

机译：以铁为催化剂，在硅上通过微波等离子体增强CVD合成碳纳米管。
6. Synthesis of Multi-Walled Carbon Nanotubes from Plastic Waste Using a Stainless-Steel CVD Reactor as Catalyst [O] . Pranav K. Tripathi, Shane Durbach, Neil J. Coville 2017

机译：不锈钢CVD反应器由塑料废料合成多壁碳纳米管
7. Catalyst nanoparticle growth dynamics and their influence on product morphology in a CVD process for continuous carbon nanotube synthesis [O] . Hoecker, C, Smail, F, Bajada, M, 2016

机译：催化剂纳米粒子生长动力学及其在连续碳纳米管合成的CVD工艺中对产物形态的影响

A NOVEL CARBON NANOTUBES SYNTHESIS CONTINUOUS PROCESS USING IRON FLOATING CATALYST ON MGO PARTICLES FOR CVD OF METHANE IN A FLUIDIZED BED REACTOR

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