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Influences of Hydrolysis Temperature and Hydrolysis Time on Titanium White Pigment via Short Sulfate Process

机译:通过短硫酸盐工艺对水解温度和水解时间对钛白色颜料的影响

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Using low concentration TiOSO_4 as titanium raw material, anatase white pigment was prepared by self seeded thermal hydrolysis route via short sulfate process. The effects of hydrolysis temperature and hydrolysis time on the structure and pigment properties of the as-prepared samples were investigated. The samples were characterized by XRD, particle size distribution and pigment properties test. The hydrolysis temperature and time had great effects on the hydrolysis rate, particle size distribution, crystal growth and particle aggregation of TiO_2, eventually determined the pigment structure and its pigment properties. The optimized hydrolysis temperature was at faint boiling point, and the hydrolysis time after second boiling point was of 2.5h. Anatase white pigment was appropriate particle size, narrow particle size distribution and good pigment properties.
机译:使用低浓度Tioso_4作为钛原料,通过短硫酸盐工艺通过自接热水解途径制备锐钛矿白颜料。研究了水解温度和水解时间对制备样品的结构和颜料特性的影响。样品的特征在于XRD,粒度分布和颜料特性试验。水解温度和时间对TiO_2的水解速率,粒度分布,晶体生长和颗粒聚集有很大的影响,最终确定颜料结构及其颜料特性。优化的水解温度是淡淡的沸点,第二沸点后的水解时间为2.5h。锐钛矿白颜料是合适的粒度,窄粒度分布和良好的颜料特性。

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