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Preparation and Properties of Starch-g-PLA with High Grafting Degree Catalyzed by Hydrochloric Acid

机译:盐酸催化高接枝度的淀粉-G-PLA的制备与性能

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Starch/lactic acid graft copolymer was attempted in situ grafting reaction of lactic grafting starch via the catalysis of hydrochloric acid. The graft copolymers of Starch and PLA had been synthesized and characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy (SEM). The synthetic condition were optimized that the weight ratios of starch with lactic acid were 1:2 when reacted for 3 hrs at 90°C in 0.6 mol/L hydrochloric acid solution. The starch-g-lactic acid copolymer can be finally obtained with graft degree of starch 65%.
机译:试图通过盐酸催化研究乳酸移植淀粉的原位接枝反应的淀粉/乳酸接枝共聚物。 通过傅里叶变换红外光谱(FT-IR),X射线衍射(XRD)和扫描电子显微镜(SEM)合成并表征淀粉和PLA的接枝共聚物。 优化合成条件,当在0.6mol / L盐酸溶液中在90℃下反应3小时时,用乳酸的淀粉的重量比为1:2。 最终可以用淀粉的接枝程度获得淀粉-G-乳酸共聚物65%。

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