The Reaction of Thiodiglycol on Metal Impregnated Carbons

机译：硫二甘醇在金属浸渍碳上的反应

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Active carbons, grade 80CTC and active carbons impregnated with cobalt (II), chromium(VI), nickel(II) and cadmium(II) and copper(II) salts, etc were saturated with the vapours of thiodiglycol (TDG) at room temperature. The carbons exposed to TDG were subjected to thermogravimetric analysis (TGA). The thermograms indicated the reactions of metal salts with the adsorbate, and was confirmed by GC-MS after extracting the reaction products from TDG exposed carbon impregnated with chromium(VI) salt and sodium hydroxide. The extractants used were dichloromethane and methanol. 1,4-oxathiane4-oxide was the reaction product of thiodiglycol on Cr(VI) impregnated carbon.

机译：室温下，80CTC活性炭和浸渍了钴（II），铬（VI），镍（II）和镉（II）和铜（II）盐等的活性炭在室温下被硫代二甘醇（TDG）的蒸气饱和。暴露于TDG的碳经过热重分析（TGA）。热谱图表明金属盐与被吸附物的反应，并且在从用铬（VI）盐和氢氧化钠浸渍的暴露于TDG的碳中提取反应产物后，通过GC-MS证实了热分析图。所使用的萃取剂是二氯甲烷和甲醇。 1,4-氧代蒽4-氧化物是硫代二甘醇在Cr（VI）浸渍的碳上的反应产物。

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《The National Conference on Advances in Carbon Materials Delhi, November, 1999》|1999年|p.57-69|共13页
会议地点 Delhi(IN)
作者
Beer Singh M.V.S. Suryanarayanan; G.K. Prasad; S. Banerjee; N.B.S.N. Rao;
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中图分类机械、仪表工业;
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The Reaction of Thiodiglycol on Metal Impregnated Carbons

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