In situ thermal oxidation route to SnO_2 nanostructures

机译：原位热氧化法制备SnO_2纳米结构

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An in situ thermal oxidation strategy was proposed for synthesizing different SnO_2 nanostructures, using our homemade SnS_2 nanoplates as a precursor. The characterization results from X-ray diffraction, energy dispersive X-ray spectroscopy, and field emission scanning electron microscope revealed that the heating temperature played an important role in the microstructure and composition of the resultant products. By heating the SnS_2 nanoplates in air at 400, 600 and 800 ℃ for 5 h, nanoplates, a mixture of nanoplates and nanoparticles, and nanoparticles of SnO_2 were synthesized, respectively. The residual S was about 2.2 mol % in the product synthesized at 400 ℃, while no residual S was detected in the products synthesized at 600 and 800 ℃.

机译：提出了一种原位热氧化策略，以自制的SnS_2纳米板为前体，合成不同的SnO_2纳米结构。 X射线衍射，能量色散X射线光谱和场发射扫描电子显微镜的表征结果表明，加热温度在所得产物的微观结构和组成中起着重要作用。通过在空气中分别在400、600和800℃下加热SnS_2纳米板5小时，分别合成了纳米板，纳米板的混合物和纳米颗粒。在400℃合成的产物中残留的S约为2.2mol％，而在600和800℃合成的产物中未检测到残留的S。

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来源
《Progress in functional materials》|2012年|150-153|共4页
会议地点 Shanghai(CN)
作者
Tian Hong Guo; Juan Li; Yong Cai Zhang; Zhan Jun Yang;
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作者单位

Key Laboratory of Environmental Material and Environmental Engineering of Jiangsu Province, College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China;

Key Laboratory of Environmental Material and Environmental Engineering of Jiangsu Province, College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China;

Key Laboratory of Environmental Material and Environmental Engineering of Jiangsu Province, College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China;

Key Laboratory of Environmental Material and Environmental Engineering of Jiangsu Province, College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China;

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原文格式 PDF
正文语种 eng
中图分类
关键词
Stannic oxide; Nanostructures; Optoelectronic materials; Powder technology;

机译：氧化锡纳米结构；光电材料；粉末技术;

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2. Large scale synthesis of flower-like SnO_2 nanostructures via a facile hydrothermal route [J] . Qiongyao He, Wen Zeng, Yang Wang, Materials Letters . 2013,第deca15期

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3. Synthesis of SnO_2 hollow nanostructures with controlled interior structures through a template-assisted hydrothermal route [J] . Zhang F., Wang K.-X., Wang X.-Y., Dalton transactions: An international journal of inorganic chemistry . 2011,第34期

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4. Hydrothermal synthesis of Ti oxide nanostructures and TiO_2:SnO_2 heterostructures applied to the photodegradation of rhodamine B [J] . Henrique A.J.L. Mourao, Waldir Avansi Junior, Caue Ribeiro Materials Chemistry and Physics . 2012,第2a3期

机译：水热法合成钛氧化物纳米结构和TiO_2：SnO_2异质结构用于罗丹明B的光降解
5. In situ thermal oxidation route to SnO_2 nanostructures [C] . Tian Hong Guo, Juan Li, Yong Cai Zhang International Conference on Optical,Electronic and Electrical Materials . 2013

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In situ thermal oxidation route to SnO_2 nanostructures

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