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Nickel Ferrite Powder Obtained by High Energy Reactive Ball Milling

机译:高能反应球磨得到的镍铁氧体粉末

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Nanocrystalline nickel ferrite powder was obtained using high energy reactive ball milling technique. Nickel oxide (NiO) and iron oxide (Fe_2O_3) powders were used as starting material. Milling was performed in air atmosphere using a planetary ball mill. Milling time was up to 30 hours. The product of milling was annealed at 350 ℃ for 4 hours in order to eliminate the internal stresses and finish the solid state reaction. X-ray diffraction analysis was used to study the nickel ferrite formation. A nanocrystallite mean size of 10 nm was found after 24 hours of milling. Using scanning electron microscopy (SEM) and energy dispersive spectrometry (EDX) the particle morphology and the chemical homogeneity were studied. It was found that the obtained product has particle size in range of micron and submicron.
机译:使用高能反应球磨技术获得了纳米晶镍铁氧体粉末。氧化镍(NiO)和氧化铁(Fe_2O_3)粉末用作原料。使用行星式球磨机在大气中进行研磨。研磨时间长达30小时。为了消除内应力并完成固相反应,将研磨产物在350℃退火4小时。 X射线衍射分析用于研究镍铁氧体的形成。研磨24小时后,发现纳米晶体的平均尺寸为10 nm。使用扫描电子显微镜(SEM)和能量色散光谱(EDX)研究了颗粒形态和化学均匀性。发现获得的产物具有在微米和亚微米范围内的粒度。

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