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Preliminary Studies and Researches on the Elaboration of Gradual Porous Sintered Structures by Powder Sedimentation

机译:粉末沉降细化渐进多孔烧结结构的初步研究

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Spherical bronze powders were used for studies the obtaining of gradual porous structures by sedimentation and sintering methods. The powder size classes above 100 urn were used for the manufacturing of the macroporous support by spreading the powder into the sintering die. Sintering was conducted in vacuum (10~(-4) Torr) at a temperature of 750 ℃ for 40 minutes. On the macroporous support a layer of fine powder fraction was deposited by gravitational sedimentation. The deposited layers were consolidated by sintering at 750 ℃ for 30 minutes. The analysis of the gradual porous layers was done using scanning electron microscopy and mercury porosimetry. The fluids viscosity influences the sedimentation velocity of particles. The height of the column directly affects the quality of porous structure. If the sedimentary column is short, the turbulences created by adding the suspension of the dispersed powder in the sedimentary tube are more harmful.
机译:球形青铜粉用于研究通过沉降​​和烧结方法获得的渐进多孔结构。通过将粉末散布到烧结模具中,将100微米以上的粉末尺寸等级用于制造大孔载体。在真空(10〜(-4)Torr)中于750℃的温度下烧结40分钟。通过重力沉降在大孔载体上沉积细粉部分层。通过在750℃下烧结30分钟来固结沉积层。使用扫描电子显微镜和水银孔率法对渐变多孔层进行分析。流体粘度影响颗粒的沉降速度。柱的高度直接影响多孔结构的质量。如果沉淀柱较短,则通过在沉淀管中添加分散粉末的悬浮液而产生的湍流更加有害。

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