In-situ x-ray diffraction study of lithium intercalation in nanostructured anatase titanium dioxide

机译：纳米结构锐钛矿型二氧化钛中锂嵌入的原位X射线衍射研究

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Electrochemical lithium intercalation in nanostructured anatase TiO_2 is investigated with in-situ X-ray diffraction. A complete and reversible phase transformation from tetragonal anatase TiO_2 to orthorhombic anatase Li_(0.5)TiO_2 is observed. The difference of the XRD spectra before and after insertion can be fitted with the lattice parameters of the two phases as fit parameters. The maximum amount of lithium that can be dissolved in anatase TiO_2 before the phase transformation occurs is found to be very small.

机译：利用原位X射线衍射研究了纳米结构锐钛矿型TiO_2中锂的电化学嵌入。观察到从四方锐钛矿型TiO_2到正交晶型锐钛型Li_（0.5）TiO_2的完全可逆的相变。插入前后的XRD光谱差异可以用两相的晶格参数拟合为拟合参数。发现在发生相变之前可溶解在锐钛矿型TiO 2中的锂的最大量非常小。

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《Symposium on Microcrystalline and Nanocrystalline Semiconductors-1998 held November 30-December 3, 1998, Boston, Massachusetts, U.S.A.》|1998年|p.337-340|共4页
会议地点 Boston MA(US)
作者
R. Van de Krol; E. A. Meulenkamp; A. Goossens; J. Schoonman;
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正文语种 eng
中图分类无线电电子学、电信技术;
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2. Electrochemical Reaction of Lithium with Nanostructured Silicon Anodes: A Study by In-Situ Synchrotron X-Ray Diffraction and Electron Energy-Loss Spectroscopy [J] . Feng Wang, Lijun Wu, Baris Key, Advanced energy materials . 2013,第10期

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3. The reaction mechanism of a complex intercalation system: In situ X-ray diffraction studies of the chemical and electrochemical lithium intercalation in Cr4TiSe8 [J] . Behrens M, Kiebach R, Ophey J, Chemistry: A European journal . 2006,第24期

机译：复杂插层系统的反应机理：Cr4TiSe8中化学和电化学锂插层的原位X射线衍射研究
4. In-situ x-ray diffraction study of lithium intercalation in nanostructured anatase titanium dioxide [C] . R. Van de Krol, E. A. Meulenkamp, A. Goossens, Symposium on microcrystalline and nanocrystalline semiconductors . 1999

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5. Synthesis and characterization of titanium dioxide thin films using scanning electron microscopy, X-ray diffraction and surface reflection FT-IR. [D] . Negron Rosado, Grimaldi Zoe. 2000

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7. DFT study of electronic and optical properties of anatase titanium dioxide tuned by nitrogen and lithium co-doping [O] . Li Qinye, Du Aijun 2016

机译：DFT研究氮和锂共掺杂调谐锐钛矿型二氧化钛的电子和光学性质

In-situ x-ray diffraction study of lithium intercalation in nanostructured anatase titanium dioxide

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