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Grain boundary structure and sliding of alumina bicrystals

机译:氧化铝双晶的晶界结构和滑动

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摘要

alumina bicrystals were fabricated by a hot joining technique at 1500 deg C in air to obtain ten kinds of [0001] symmetric tilt grain boundaries which included small angle, CSL and high angle grain boundaries. Their grain boundary structures were investigated by high-resolution electron microscopy (HREM), and the respoective grain boundary energies were systematically measured by a thermal grooving technique. It was found that grain boundary energy strongly depended on the grain boundary characters, e.g., there were large energy cusps at low sum CSL grain boundaries. But, main part of grain boundary energy is likely to be due to the strain energy around the grain boundary, and he contribution of atomic configuration is not sl large. Small angle grain boundaries were consisted of an array of partial dislocation with Burgers vector of 1/3[1100] to form the stacking faults between the dislocations. The behavior of grain boundary sliding was also investigated for typical grain boundaries by high-temperature creep test at 1400 deg C. As the result, the occurrence of grain boundary sliding was found to depend on the grain boundary atomic structure.
机译:通过在空气中于1500℃下的热连接技术制造氧化铝双晶,以获得十种[0001]对称倾斜晶界,包括小角度,CSL和大角度晶界。通过高分辨率电子显微镜(HREM)研究了它们的晶界结构,并通过热切槽技术系统地测量了反应性晶界能。发现晶界能强烈地依赖于晶界特征,例如,在低和CSL晶界处具有大的能量尖端。但是,晶界能的主要部分可能是由于晶界周围的应变能引起的,原子构型的贡献并不大。小角度晶界由部分位错的阵列组成,其Burgers矢量为1/3 [1100],从而形成位错之间的堆垛层错。还通过在1400℃下的高温蠕变试验研究了典型晶界的晶界滑动行为。结果,发现晶界滑动的发生与晶界原子结构有关。

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