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Effects of microalloying on hot-rolled and cold-rolled Q&P steels.

机译:微合金化对热轧和冷轧Q&P钢的影响。

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摘要

Third generation advanced high strength steels (AHSS) have been a major focus in steel development over the last decade. The premise of these types of steel is based on the potential to obtain excellent combinations of strength and ductility with low-alloy compositions by forming mixed microstructures containing retained austenite (RA). The development of heat treatments able to achieve the desired structures and properties, such as quenching and partitioning (Q&P) steels, is driven by new requirements to increase vehicle fuel economy by reducing overall weight while maintaining safety and crashworthiness.;Microalloying additions of niobium (Nb) and vanadium (V) in sheet products are known to provide strengthening via grain refinement and precipitation hardening and may influence RA volume fraction and transformation behavior. Additions of microalloying elements in Q&P steels have not been extensively studied to date, however. The objective of the present study was to begin to understand the potential roles of Nb and V in hot-rolled and cold-rolled Q&P steel. For that, a common Q&P steel composition was selected as a Base alloy with 0.2C-1.5Si-2.0Mn (wt. %). Two alloys with an addition of Nb (0.02 and 0.04 wt. %) and one with an addition of V (0.06 wt. %) to the Base alloy were investigated. Both hot-rolled and cold-rolled/annealed Q&P simulations were conducted.;In the hot-rolled Q&P study, thermomechanical processing was simulated via hot torsion testing in a GleebleRTM 3500, and four coiling temperatures (CT) were chosen. Microstructural evaluation (including RA measurements via electron backscattered diffraction - EBSD) and hardness measurements were performed for all alloys and coiling conditions. The analysis showed that Nb additions led to overall refinement of the prior microstructure. Maximum RA fractions were measured at the 375 °C CT, and microalloying was associated with increased RA in this condition when compared to the Base alloy. A change in austenite morphology from lath-like to blocky with increasing CT was observed. Hardness generally increased with decreasing CT, consistent with the increased fraction of harder phases in the microstructure.;For the cold-rolled Q&P study, several combinations of quenching temperature (QT), partitioning temperature (PT), and partitioning time (t p) were examined using heat treatments in salt baths. Uniaxial tensile tests and RA measurements via x-ray diffraction (XRD) were performed for all alloys and heat treatment conditions. Scanning electron microscope (SEM) imaging and EBSD were conducted for a few select conditions. In terms of microstructure, Nb promoted an extensive refinement of the prior austenite grain size. Additions of V and Nb also seemed to affect the morphology of the microstructural constituents. It was observed that V generally increased austenite fractions at lower t p's, and the Nb-containing alloys had greater austenite fractions in most instances when compared to the Base alloy. Carbon content in austenite was usually increased or maintained with additions of Nb and V. In terms of mechanical properties, V slightly improved strength and elongation when compared to the Base alloy for most conditions. Niobium additions were somewhat more effective in improving ductility.
机译:在过去的十年中,第三代高强度高强度钢(AHSS)一直是钢发展的主要重点。这些钢的前提是通过形成含有残留奥氏体(RA)的混合微观结构,从而获得低强度合金成分的强度和延展性的极好组合。新的要求推动了能够实现所需结构和性能的热处理的发展,例如淬火和分隔(Q&P)钢,这些新要求通过降低总体重量同时保持安全性和耐撞性来提高车辆燃油经济性。已知片材产品中的Nb)和钒(V)可通过晶粒细化和沉淀硬化来提供强化作用,并可能影响RA体积分数和相变行为。迄今为止,尚未对Q&P钢中的微合金元素进行广泛的研究。本研究的目的是开始了解Nb和V在热轧和冷轧Q&P钢中的潜在作用。为此,选择一种常见的Q&P钢成分作为具有0.2C-1.5Si-2.0Mn(重量%)的基础合金。研究了两种添加了Nb(0.02和0.04 wt。%)的合金和一种添加了V(0.06 wt。%)的合金。进行了热轧和冷轧/退火Q&P模拟;在热轧Q&P研究中,通过在GleebleRTM 3500中进行热扭转测试对热机械加工进行了模拟,并选择了四个卷取温度(CT)。对所有合金和卷取条件进行了微结构评估(包括通过电子背散射衍射进行的RA测量-EBSD)和硬度测量。分析表明,添加Nb可以使先前的微观结构得到全面改善。在375°C CT下测量了最大的RA分数,与母材合金相比,在这种条件下微合金化与RA的增加有关。随着CT的增加,观察到奥氏体形态从板条状变为块状。硬度通常随着CT的降低而增加,这与显微组织中较硬相的分数增加相一致。;对于冷轧Q&P研究,淬火温度(QT),分配温度(PT)和分配时间(tp)的几种组合是在盐浴中使用热处理进行了检查。对所有合金和热处理条件进行了单轴拉伸试验和通过X射线衍射(XRD)进行的RA测量。在一些选定条件下进行了扫描电子显微镜(SEM)成像和EBSD。就微观结构而言,Nb促进了先前奥氏体晶粒尺寸的广泛细化。 V和Nb的添加似乎也影响了微结构成分的形态。观察到,在较低的t p时,V通常会增加奥氏体分数,并且与基础合金相比,在大多数情况下,含Nb的合金的奥氏体分数更高。通常通过添加Nb和V来增加或保持奥氏体中的碳含量。就机械性能而言,在大多数情况下,与基础合金相比,V略微提高了强度和伸长率。铌的添加在改善延展性方面更有效。

著录项

  • 作者单位

    Colorado School of Mines.;

  • 授予单位 Colorado School of Mines.;
  • 学科 Materials science.;Mechanics.
  • 学位 M.S.
  • 年度 2016
  • 页码 137 p.
  • 总页数 137
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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