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An assessment of severe plastic deformation for producing submicrocrystalline copper.

机译:对生产亚微晶铜的严重塑性变形的评估。

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摘要

This project is a critical assessment of the mechanical properties and structure of metals subjected to severe plastic deformation (SPD) processing. The project focuses on equal channel angular forging and on copper as the model material. Numerous reports have been made that SPD methods are capable of producing metals and alloys with a sub-microcrystalline grain size which have desirable mechanical properties and an unusual grain boundary structure. Although other possibilities were kept in mind, the experiments were conducted with the expectation that traditional metallurgical principles would explain the results. This expectation has been fulfilled. Briefly, the elastic behavior of SPD Cu is modified by texture; the tensile behavior is characterized by saturation and early plastic instability; the fatigue performance is marked by cyclic softening; and the creep behavior is dictated by microstructural instability. The microstructure is indeed very fine, having a cell size of ≈0.25 μm with boundaries which are indistinguishable from the original grain boundaries at first glance. However, through careful TEM examination it was determined that there is a more significant population of low angle boundaries in the SPD material than in an annealed polycrystal. Along with diffusion data obtained from creep experiments, this difference provides an explanation for rapid “grain” growth in terms of existing models of subgrain growth and coalescence. Finally, by using polycrystal plasticity simulations to model the equal channel angular forging process, the condition of simple shear has been verified and an accurate prediction of texture has been achieved.
机译:该项目是对遭受严重塑性变形(SPD)处理的金属的机械性能和结构的重要评估。该项目侧重于等径角锻造,并以铜为模型材料。已经有许多报道说SPD方法能够生产具有亚微晶晶粒尺寸的金属和合金,这些金属和合金具有理想的机械性能和不寻常的晶界结构。尽管记住了其他可能性,但进行实验时希望传统的冶金原理可以解释结果。这个期望已经实现。简而言之,SPD Cu的弹性行为会被织构改变。拉伸行为的特征是饱和和早期塑性不稳定性。疲劳性能以循环软化为特征;蠕变行为由微观结构的不稳定性决定。显微组织确实非常精细,单元尺寸约为0.25μm,其边界乍一看与原始晶界没有区别。但是,通过仔细的TEM检查,可以确定SPD材料中的低角度边界比退火多晶中的人口大得多。与从蠕变实验获得的扩散数据一起,这种差异为现有的亚晶粒生长和合并模型提供了快速“晶粒”生长的解释。最后,通过多晶塑性模拟对等通道角锻造过程进行建模,验证了简单剪切的条件,并获得了准确的织构预测。

著录项

  • 作者

    Agnew, Sean Rogers.;

  • 作者单位

    Northwestern University.;

  • 授予单位 Northwestern University.;
  • 学科 Engineering Materials Science.; Engineering Metallurgy.
  • 学位 Ph.D.
  • 年度 1998
  • 页码 132 p.
  • 总页数 132
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 工程材料学;冶金工业;
  • 关键词

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