以过硫酸钾为引发剂,微波辐射,双原位合成了纳米银/聚丙烯酰胺(PAM),纳米银/聚2-丙烯酰胺基-2-甲基丙磺酸(PAMPS)的复合物.TEM和XRD的结果表明了两种体系中都有纳米银的生成但具有不同形貌结构；FTIR结果表明在两种体系中分别合成了聚丙烯酰胺和聚2-丙烯酰胺基-2-甲基丙磺酸；XPS结果表明了聚合物中的N元素和Ag元素之间有相互作用.%Nano-silver/poly(2-acrylamido-2-methylpropanesulfonic acid) (PAMPS) and Nano-silver/Polyacrylamide(PAM)composite materials were successfully synthesized bi-in situ from silver nitrate solution with acrylamide( AM)or 2-acrylamido-2-methylpro-panesulfonic acid( AMPS) monomer under microwave irradiation,with potassium persulfate as initiator. TEM and XRD indicated the presence of nano silver with different microstructure in two systems. FTIR showed that poly(2-acrylamido-2-methylpropanesulfonic acid)and Polyacrylamide were successfully synthesized;XPS suggested that niteogen had interaction with silver.
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