报道了4-氨基-1，2，4-三唑-5-酮(ATO)的制备方法，通过DSC热分析研究了其常规热分解，通过采用T-jump/FT-IR技术对ATO的快速热分解过程进行了研究，提出了其主要气相产物的浓度变化曲线。%4-Amino-1，2，4-triazol-5-one(ATO) was prepared in this paper. Its conventional thermal decomposition was described by DSC technology. The flash pyrolysis of ATO was investigated by T-jump/FT-IR spectroscopy. The concentration change curve of the main gaseous remains was put forward.
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