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Preparation of copper nanoparticles by chemical reduction method using potassium borohydride

机译:硼氢化钾化学还原法制备铜纳米粒子

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摘要

High dispersive copper nanoparticles were prepared by chemical reduction method using potassium borohydride as reducing agent.The effects of reactant ratio,concentration of CuSO4,reaction temperature,and dispersant on the size of product and conversion rate were studied.The morphologies of copper nanoparticles were characterized by scanning electron microscopy.The results show that the optimum process conditions are as follows:the molar ratio of KBH4 to CuSO4 is 0.75(3:4),concentration of CuSO4 is 0.4 mol/L,reaction temperature is 30℃,and dispersant is n-butyl alcohol.The average particles size of copper powders with spherical shape gained is about 100 nm.
机译:以硼氢化钾为还原剂,通过化学还原法制备了高分散铜纳米颗粒。研究了反应物配比,CuSO4浓度,反应温度和分散剂对产物尺寸和转化率的影响。表征了铜纳米颗粒的形貌结果表明,最佳工艺条件为:KBH4与CuSO4的摩尔比为0.75(3:4),CuSO4的浓度为0.4 mol / L,反应温度为30℃,分散剂为正丁醇:获得的球形铜粉的平均粒径约为100 nm。

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