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Preparation and characterization of ultrafine zinc oxide powder by hydrothermal method

机译:水热法制备超细氧化锌粉及其表征

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With Zinc acetate and sodium hydroxide as raw materials,while polyethylene glycol employed as dispersant agent, ultrafine zinc oxide powder was synthesized by hydrothermal method.Influence of NaOH concentration on morphology of ZnO powder was studied.The as-synthesized ZnO powder looked like flower cluster and consisted of microrods with hexagonal morphologies.The crystal structure and optical property of the as-prepared powder were also characterized using XRD,UV-visible absorption spectrum and photoluminescence spectrum.The results indicate that ZnO powder is of hexagonal wurtzite structure and well crystallized with high purity.There is a strong excitation absorption peak at 300 nm in UV-visible absorption spectrum and blue shift exists obviously.The optical property of ZnO powder is excellent.
机译:以乙酸锌和氢氧化钠为原料,以聚乙二醇为分散剂,水热法合成了超细氧化锌粉,研究了NaOH浓度对ZnO粉形貌的影响,合成后的ZnO粉呈花簇状用XRD,紫外可见吸收光谱和光致发光光谱对所制备粉末的晶体结构和光学性能进行了表征。 ZnO粉末的光学性能优异,在300 nm处有很强的激发吸收峰,并且有明显的蓝移现象。

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