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Response surface design for nickel recovery from laterite by sulfation-roasting-leaching process

机译:通过硫酸盐焙烧-浸出工艺从红土中回收镍的响应面设计

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摘要

The present study deals with the nickel extraction and iron dissolution from nickeliferous laterite by a process of sulfation-roasting-leaching.To optimize the roasting process,response surface methodology(RSM)was utilized which employed two-level and two-factor full factorial central composite design(CCD).The factors of roasting temperature and time were studied. Experiments were carried out for fitting two non-linear regression models of nickel extraction and iron dissolution.Predicted values obtained were close to experimental values,indicating the suitability of the models.Three-dimensional surface plots and contour plot were helpful to predicting the results by performing only limited set of experiments.An area of nickel extraction from 75%to 78% and iron dissolution from 5%to 10%is obtained by an overlaid contour plot.The samples roasted at different temperatures and for different durations were characterized by XRD,which show a good agreement to iron dissolution analysis.
机译:本研究通过硫酸化-焙烧-浸出工艺处理镍红土中的镍和铁的溶出。为优化焙烧工艺,采用响应面法(RSM),该方法采用两级两因素全因子中心法。研究了焙烧温度和时间的影响因素。进行了两个拟合镍提取和铁溶解的非线性回归模型的实验,得出的预测值与实验值接近,表明模型的适用性。三维表面图和轮廓图有助于通过以下方法预测结果通过重叠等高线图获得了镍提取率从75%到78%以及铁溶出度从5%到10%的区域。通过XRD对在不同温度和持续时间下焙烧的样品进行了表征,与铁溶出分析显示出很好的一致性。

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