Undercooled melt of Ge_(73.7)Ni_(26.3) alloy sample floated on B_(2)O_(3 ) melt was subjected to sputtering-deposition of Ni clusters on cooling to induce solidification.The initial temperature of solidification was 975 K.Its undercoolingΔT was 134 K with respect to the melting temperature of the primary phase Ge.On the cooling curve existed dual recalescences representing the transformation of the primary phase(Ge)and the eutectics(Ge+GeNi)respectively.But for the sample unsputtered,only a single exothermic peak presented on the cooling curve with the initial solidification temperature of 904K and undercooling of 205K.Careful observation of the microstructure proved that the Ge phase primarily formed in the sputtering experiment was now formed together with the formation of the eutectics in the experiment without sputtering.
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机译:A comparative EBSP study of microstructure and microtexture formation from undercooled Ni_(99)B_1 melts solidified on an electrostatic levitator and an electromagnetic levitator