The MWD-ICP-AES was used to determinate microelements from abalone in Sanya, including Cu, Zn, Pb, Cd, Mn, Cr, Ni, Co, Mo, Ba, V.The method of sample treatment by MWD had some advantages:processing thoroughly, less loss, less acid consumption, without special monitoring, shortened digestion time, improved test efficiency. Comparing with the traditional analysis method, the method of determination by ICP-AES had some advantages also:more convenient and quick operation, wider linear range, lower detection lim-it, and higher recovery rate.%以三亚鲍鱼为原料,采用微波消解技术与电感耦合等离子发射光谱(ICP-AES)法相结合测定样品微量元素方法,测定鲍鱼中Cu、Zn、Pb、Cd、Mn、Cr、Ni、Co、Mo、Ba、V 11种元素含量.以微波消解法对鲍鱼样品进行处理,样品处理彻底,损失量少,耗酸少,消解过程无需专人看管,消解时间缩短,提高试验效率;与传统分析方法相比,ICP-AES法测定操作更为方便快捷,线性范围较宽,检出限更低,精密度更高,加标回收率高.
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