An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters

Feng Zhu; Zhijian Yao; Wenliang Ji; Deye Liu; Hao Zhang; Aimin Li; Zongli Huo; Qing Zhou

首页> 中文期刊> 《中国环境科学与工程前沿：英文版》 >An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters

An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters

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In this study,a hydrophilic resin named GCHM was fabricated based on poly(N-vinyl pyrrolidone-codivinylbenzene),characterized,and applied as a solid-phase extraction(SPE)material.Up to 44 pharmaceuticals and personal care products(PPCPs)belonging to 10 classes were recovered in environmental water samples.Different variables affecting extraction,such as adsorbent amount,sample pH,and loading speed,were optimized.Under optimal conditions,the average absolute recovgy of 44 PPCPs was 75.6%using GCHM,indicating a better performance than the commercial Oasis^HLB.SPE with home-made hydrophilic polymeric sorbent followed by ultra-performance liquid chromatography and tandem mass spectrometry was validated,and the method achieved good linearity(r2>0.991,for all analytes).In addition,the method detection limits of target compounds ranged from 0.03 to 0.6 ng/L.The developed method was applied to determine PPCPs in 10 environmental water samples taken from the Yangtze River,Huaihe River,and Taihu Lake,1 groundwater sample from Changzhou in Jiangsu Province,1 wastewater sample from Xiamen and 2 seawater samples from the Jiulong River in Fujian Province,China.In these samples,22 compounds were determined at levels ranging from 0.5 to 1590 ng/L.

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《中国环境科学与工程前沿：英文版》 |2020年第3期|P.177-187|共11页
作者
Feng Zhu; Zhijian Yao; Wenliang Ji; Deye Liu; Hao Zhang; Aimin Li; Zongli Huo; Qing Zhou;
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作者单位

Jiangsu Provincial Center for Disease Control and Prevention Nanjing 210009 China;

State Key Laboratory of Pollution Control and Resource Reuse School of the Environment Nanjing University Nanjing 210023 ChinaJiangsu Guochuang Enviro-protection Technology Co.Ltd. No.19 Changqing Avenue Nanjing 211100 China;

Jiangsu Provincial Center for Disease Control and Prevention Nanjing 210009 China;

Jiangsu Provincial Center for Disease Control and Prevention Nanjing 210009 China;

Jiangsu Provincial Center for Disease Control and Prevention Nanjing 210009 China;

State Key Laboratory of Pollution Control and Resource Reuse School of the Environment Nanjing University Nanjing 210023 China;

Jiangsu Provincial Center for Disease Control and Prevention Nanjing 210009 China;

State Key Laboratory of Pollution Control and Resource Reuse School of the Environment Nanjing University Nanjing 210023 ChinaJiangsu Guochuang Enviro-protection Technology Co.Ltd. No.19 Changqing Avenue Nanjing 211100 China;

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原文格式 PDF
正文语种 chi
中图分类中国工业经济;
关键词
Hydrophilic resin; Solid phase extraction; Pharmaceuticals and personal care product; Ultra-performance liquid chromatography; and tandem mass spectrometry; Environmental water;

机译：亲水性树脂;固相萃取;药物和个人护理产品;超高效液相色谱;串联质谱;环境水;

An efficient resin for solid-phase extraction and determination by UPLCMS/MS of 44 pharmaceutical personal care products in environmental waters

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