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《海南医科大学学报(英文版)》
>The study on the methods of testing the sulphuric acid and the phosphoric acid in the air in workshops at the same time by chromatography of ions
The study on the methods of testing the sulphuric acid and the phosphoric acid in the air in workshops at the same time by chromatography of ions
Objective:To discuss the method and result of testing the sulphuric acid and the phosphoric acid in the air in workshops at the same time by chromatography of ions.Method:to measure the sulphuric acid and the phosphoric acid in the air in workshops by adopting chromatography of ions. During the experiment, collect the sulphuric acid and the phosphoric acid in the air by using porous glass plates and put them into ultrapure water, or by using microporous filtering film, adopting ultrasonic elution with ultrapure water, testing them with ion chromatograph after filtering through a 0.2 μm microporous filtering film. The operating conditions of chromatography of ions includes Type Ionpac AS19 separator column (4×250 mm), ASRS300 (4 mm) anion suppressor, Type Ionpac AG19 guard column, KOH eluent and conductivity detector.Result: The testing the sulphuric acid and the phosphoric acid at the same time through chromatography of ions turns out high resolution, good linearity with the correlation over 0.999. The accuracy can be controlled between 1.6%-5.5% under the testing; the percentage of accuracy can be guaranteed between 92%-107% with high sampling and analysis efficiency.Conclusion: The method can turn out ideal results by testing the sulphuric acid and the phosphoric acid at the same time. It is simple operations, Sensitive and accurate. It is worth being used widely.
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