首页> 中文期刊> 《等离子体科学和技术:英文版》 >The Role of Nanodispersed Nitrides in the Sintering of Silicon Nitride Ceramics

The Role of Nanodispersed Nitrides in the Sintering of Silicon Nitride Ceramics

         

摘要

The synthesis of ceramics based on silicon nitride using nanopowders of TiN andSi_3N_4 as additives was studied. The ceramic compositions were pressurelessly sintered under nitrogenatmosphere at different temperatures (1550℃, 1650℃ and 1750℃) with a heating rateof 10℃/min and a holding time of 2 h. The nanodispersed nitrides (NDN) were produced byelectric-arc plasma synthesis and characterized. The ceramic composites obtained with nanoparticlesof 1wt% to 5wt% TiN and 20wt% Si_3N_4 were characterized by scanning electron microscopy(SEM), atom force microscopy (AFM) and energy-dispersive spectrometry (EDX). The effect ofthe addition of nanodispersed powders on the mechanical properties and microstructure of Si_3N_4ceramics was investigated.

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