Aimed at high content of valuable metals, complicated composition, difficult to separation of precious metals six component alloy wastes, the present paper proposed a new technology of high efficient separation and purification. Using fragmentation technology realizes fast dissolution of palladium, silver, copper and zinc in the wastes, and high efficient and complete separation of them from gold and platinum; using evaporation thermal decomposition technology of mixed solution produced by nitric acid dissolving palladium, silver, copper and zinc, complete and high efficient separation of silver from palladium was realized; by control of solution acidity, using hydrazine reduction method, high efficient and complete separation of gold from platinum was realized. Using this new technology, the recovery rates of palladium and silver are above 99%, and gold and platinum above 98%, the grade of pure metals are above 99.95%.
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