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均匀设计在活性碘化铑制备中的应用

         

摘要

研究了各种因素对合成碘化铑的影响.采用均匀实验方法对试验进行设计以及数据优化处理,确定合成碘化铑反应的最佳值因素水平数,即:反应温度为500℃、反应时间为30 h、碘铑比为13的条件下,铑的转化率最高达65%.%The effects of several tactors on the preparation of rhodium iodide were investigated in this article. The experiments were designed using the uniform design method, and data were optimized. The optimum factor levels for synthesis of rhodium iodide were determined as follows: reaction temperature is 500℃,reaction time is 30 h,I2/Rh is 13,Under these conditions, the highest convert rate of rhodium is 65%.

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