首页> 美国卫生研究院文献>Acta Biomaterialia Odontologica Scandinavica >A novel etching technique for surface treatment of zirconia ceramics to improve adhesion of resin-based luting cements
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A novel etching technique for surface treatment of zirconia ceramics to improve adhesion of resin-based luting cements

机译:一种用于氧化锆陶瓷表面处理的新型蚀刻技术可提高树脂基胶泥的附着力

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摘要

>Objectives: Bonding of zirconia crowns and bridges to abutments is important, not only bonding of the thin resin layer to the abutment, but also bonding to the zirconia ceramic is crucial. Both mechanical and chemical adhesion are desired. Mechanical retention of dental porcelain achieved by etching with moderately concentrated hydrofluoric acid is not possible with zirconia ceramics.The purpose of this study was to show that etching is possible with relative low melting fluoride compounds such as ammonium hydrogen difluoride and potassium hydrogen difluoride. >Materials and methods: Before melting, the fluorides can be introduced as powders or as aqueous slurries to the contact surfaces of the zirconia. After melting, the yttria-stabilized zirconia surface revealed a surface similar to an HF-etched dental feldspathic porcelain surface. Shear bond testing (n = 10) was performed with zirconia attached to zirconia with the Duo-Link composite luting cement (Bisco) after treatment of the etched zirconia surfaces with Bis-Silane (Bisco) and the Porcelain Bonding Resin (Bisco). >Results: Values for adhesive strength (mean ± standard deviation) after melt etching of the surfaces with initially dry powders were for K[FHF], (31.2 ± 7.5) MPa and for NH4[FHF] (31.0 ± 11.8) MPa. When initially aqueous slurries were applied, the values were for K[FHF] (42.7 ± 12.7) MPa and for NH4[FHF] (40.3 ± 10.0) MPa. >Conclusion: Good adhesion to zirconia can be achieved by a procedure including etching with selected melted fluoride compounds.
机译:>目标:氧化锆冠和桥与基台的粘接很重要,不仅薄树脂层与基台的粘接,而且与氧化锆陶瓷的粘接也至关重要。机械和化学粘附都是需要的。氧化锆陶瓷不可能通过用中等浓度的氢氟酸蚀刻来实现对牙科瓷器的机械固位。本研究的目的是证明使用相对较低熔点的氟化物(例如二氟化氢铵和二氟化氢钾)可以进行蚀刻。 >材料和方法:在熔化之前,氟化物可以粉末形式或水性浆料形式引入到氧化锆的接触表面。熔化后,氧化钇稳定的氧化锆表面显示出与HF蚀刻的牙齿长石瓷表面相似的表面。在用Bis-Silane(Bisco)和瓷结合树脂(Bisco)处理蚀刻后的氧化锆表面后,用Duo-Link复合胶凝水泥(Bisco)在附着有氧化锆的氧化锆上进行了剪切粘结试验(n = 10)。 >结果:最初用干粉对表面进行熔融蚀刻后的粘合强度(平均值±标准偏差)为K [FHF],(31.2±7.5)MPa和NH4 [FHF](31.0) ±11.8)兆帕最初使用水性浆料时,K [FHF](42.7±12.7)MPa和NH4 [FHF](40.3±10.0)MPa的值。 >结论:通过包括使用选定的熔融氟化物蚀刻的工艺,可以实现对氧化锆的良好附着力。

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