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Synthesis and Characterization of Nano Boron Nitride Reinforced Magnesium Composites Produced by the Microwave Sintering Method

机译:微波烧结法制备纳米氮化硼增强镁复合材料的表征

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摘要

In this study, magnesium composites with nano-size boron nitride (BN) particulates of varying contents were synthesized using the powder metallurgy (PM) technique incorporating microwave-assisted two-directional sintering followed by hot extrusion. The effect of nano-BN addition on the microstructural and the mechanical behavior of the developed Mg/BN composites were studied in comparison with pure Mg using the structure-property correlation. Microstructural characterization revealed uniform distribution of nano-BN particulates and marginal grain refinement. The coefficient of thermal expansion (CTE) value of the magnesium matrix was improved with the addition of nano-sized BN particulates. The results of XRD studies indicate basal texture weakening with an increase in nano-BN addition. The composites showed improved mechanical properties measured under micro-indentation, tension and compression loading. While the tensile yield strength improvement was marginal, a significant increase in compressive yield strength was observed. This resulted in the reduction of tension-compression yield asymmetry and can be attributed to the weakening of the strong basal texture.
机译:在这项研究中,使用粉末冶金(PM)技术结合了微波辅助双向烧结和热挤压技术,合成了具有不同含量的纳米级氮化硼(BN)颗粒的镁复合材料。利用结构-性质相关性,研究了纳米BN添加对所开发的Mg / BN复合材料的微观结构和力学行为的影响,并与纯Mg进行了比较。微观结构表征揭示了纳米BN颗粒的均匀分布和边缘晶粒细化。镁基体的热膨胀系数(CTE)值通过添加纳米级BN颗粒得以改善。 XRD研究的结果表明,随着纳米BN添加量的增加,基础纹理减弱。该复合材料在微压痕,拉伸和压缩载荷下显示出改善的机械性能。尽管抗拉屈服强度的改善很小,但观察到抗压屈服强度的显着增加。这导致张力-压缩屈服不对称性的降低,并且可以归因于强基部质地的减弱。

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