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X-ray diffraction and TGA kinetic analyses for chemical looping combustion applications

机译:X射线衍射和TGA动力学分析用于化学循环燃烧应用

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摘要

Synthesis and characterization of supported metal-based oxygen carriers were carried out to provide information related to the use of oxygen carriers for chemical looping combustion processes. The Cu, Co, Fe, Ni metals supported with Al2O3, CeO2, TiO2, ZrO2 were prepared using the wetness impregnation technique. Then, the X-ray Diffraction (XRD) characterization of oxidized and reduced samples was obtained and presented. The kinetic analysis using Thermogravimetric analyzer (TGA) of the synthesized samples was conducted. The kinetics of reduction reaction of all samples were estimated and explained.
机译:进行了负载型金属基氧载体的合成和表征,以提供与在化学循环燃烧过程中使用氧载体有关的信息。采用湿法浸渍法制备了以Al2O3,CeO2,TiO2,ZrO2负载的Cu,Co,Fe,Ni金属。然后,获得并呈现了氧化和还原样品的X射线衍射(XRD)表征。使用热重分析仪(TGA)对合成样品进行动力学分析。估计并解释了所有样品的还原反应动力学。

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