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Automated electron diffraction tomography – development and applications

机译:自动化电子衍射层析成像技术的开发与应用

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摘要

Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.
机译:从自动电子衍射层析成像(ADT)的发展开始,电子衍射层析成像(EDT)引起了越来越多的兴趣,该技术使得能够从适合从头算结构分析的纳米尺寸晶体中收集三维电子衍射数据。提供了对ADT方法的基本描述,该方法现已被认为是一种可靠的既定方法,并提供了它的特殊功能和对不同透射电子显微镜的普遍适用性。此外,还证明了ADT在具有和不具有特殊晶体学特征(例如孪晶,调制和无序)的单纳米晶体的晶体结构分析中的可用性。

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