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Structural vibrational and optical studies on semiorganic crystals of boric acid potassium acetate

机译:硼酸乙酸钾半有机晶体的结构振动和光学研究

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摘要

A semiorganic crystal of Boricacid potassium acetate has been grown by low temperature solution growth technique at room temperature using deionized water as a solvent. The crystalline nature of the compound was confirmed by the sharp and well defined peaks observed from the powder X-ray diffraction pattern. By single crystal X-ray diffraction method, the structure of the grown crystal has been studied. The Boric acid Potassium Acetate (BAPA) crystal has good optical transmittance in the entire UV visible region. FT-IR and FT-Raman spectral studies were performed to identify the vibrations of functional groups. The mechanical strength of the grown crystal was determined by Vicker's micro hardness test. Photoluminescence study was carried out on the crystal. The SHG study represents the nonlinear optical efficiency of the crystal.
机译:硼酸乙酸钾的半有机晶体已经通过低温溶液生长技术在室温下使用去离子水作为溶剂来生长。由粉末X射线衍射图观察到的尖锐且界限分明的峰证实了该化合物的结晶性质。通过单晶X射线衍射法,已经研究了生长的晶体的结构。硼酸乙酸钾(BAPA)晶体在整个UV可见光区域具有良好的透光率。进行了FT-IR和FT-拉曼光谱研究,以识别官能团的振动。生长的晶体的机械强度通过维氏显微硬度测试确定。对晶体进行了光致发光研究。 SHG研究代表了晶体的非线性光学效率。

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