Investigation of the Most Effective Cotton Digestion Procedure

Iva Rezic

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Investigation of the Most Effective Cotton Digestion Procedure

机译：最有效的棉花消化程序的调查

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Three cotton digestion procedures were tested to determine major, minor, and trace elements by inductively coupled plasma atomic emission spectrometry. Homogenized samples were subjected to dry ashing, open-vessel digestion, and microwave digestion before analysis for the presence of 28 elements. Best recoveries of all elements, especially for Cd and Co analysis, occured after the microwave digestion procedure. Dry ashing was the best method for determining As, K, Mg, Mn and Na, while open-vessel digestion was best for Al, Be, Ca, and Sb analysis. Digestion method accuracies were estimated by analysis of a certified reference material. Very good agreement between certified and experimental values was found for the majority of elements investigated.

机译：通过电感耦合等离子体原子发射光谱法测试了三种棉花消化程序，以确定主要，次要和痕量元素。对均质的样品进行干灰化，开放式容器消化和微波消化，然后分析是否存在28种元素。微波消解后，所有元素的回收率最高，尤其是对于Cd和Co分析而言。干灰化是确定As，K，Mg，Mn和Na的最佳方法，而开孔消解是Al，Be，Ca和Sb分析的最佳方法。消化方法的准确性是通过对标准参考物质的分析来估计的。对于所研究的大多数元素，已证明认证值与实验值之间具有很好的一致性。

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来源
《AATCC review》 |2011年第1期|p.58-63|共6页
作者
Iva Rezic;
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作者单位

University of Zagreb, Faculty of Textile Technology, Prilaz Baruna Filipovica 28a,10000 Zagreb, Croatia;

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原文格式 PDF
正文语种 eng
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关键词
cotton; digestion; ICP-AES; trace elements;

机译：棉;消化;ICP-AES;微量元素;

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Investigation of the Most Effective Cotton Digestion Procedure

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