Alternating Silica/Polymer Multilayer Hybrid Microspheres Templates for Double-shelled Polymer and Inorganic Hollow Microstructures

Guoliang Li† Qin Shi† S. J. Yuan† K. G. Neoh† E. T. Kang† and Xinlin Yang‡

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Alternating Silica/Polymer Multilayer Hybrid Microspheres Templates for Double-shelled Polymer and Inorganic Hollow Microstructures

机译：双壳聚合物和无机空心微结构的交替二氧化硅/聚合物多层杂化微球模板

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Alternating silica/polymer tetra- and penta-layer hybrid microspheres were first prepared via combined inorganic sol−gel reaction and distillation-precipitation polymerization. pH-responsive poly(methacrylic acid) (PMAA) hollow microspheres with asymmetric double-shells were produced after HF etching of the silica layers in the SiO₂/PMAA tetra-layer microspheres with different degrees of cross-linking in the two PMAA layers. On the other hand, silica “core−double shell” hollow microspheres were obtained by calcination of the alternating silica/PMAA penta-layer microspheres. The resulting hollow polymer and silica microspheres with hierarchical structures were characterized by field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), energy-dispersive X-ray (EDX) analysis, dynamic laser scattering (DLS), and confocal laser scanning microscopy (CLSM) measurements.

机译：交替的二氧化硅/聚合物四层和五层杂化微球首先通过组合的无机溶胶-凝胶反应和蒸馏-沉淀聚合反应制备。在对具有不同交叉度的SiO _{2 / PMAA四层微球中的二氧化硅层进行HF蚀刻之后，制得了具有不对称双壳的pH响应的聚甲基丙烯酸（PMAA）中空微球。在两个PMAA层中链接。另一方面，通过交替二氧化硅/ PMAA五层微球的煅烧获得了二氧化硅“核-双壳”中空微球。通过场发射扫描电子显微镜（FESEM），透射电子显微镜（TEM），能量色散X射线（EDX）分析，动态激光散射（DLS）和共聚焦来表征具有分层结构的所得空心聚合物和二氧化硅微球激光扫描显微镜（CLSM）测量。}

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《American Chemical Society》 |2010年第4期|p.1309-1317|共9页
作者
Guoliang Li† Qin Shi† S. J. Yuan† K. G. Neoh† E. T. Kang† and Xinlin Yang‡;
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Guoliang Li† Qin Shi† S. J. Yuan† K. G. Neoh† E. T. Kang† and Xinlin Yang‡;

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1. Alternating Silica/Polymer Multilayer Hybrid Microspheres Templates for Double-shelled Polymer and Inorganic Hollow Microstructures [J] . Guoliang Li, Qin Shi, S. J. Yuan Chemistry of Materials: A Publication of the American Chemistry Society . 2010,第4期

机译：双壳聚合物和无机空心微结构的交替二氧化硅/聚合物多层杂化微球模板
2. Preparation of silica/polymer hybrid microspheres and the corresponding hollow polymer microspheres with functional groups [J] . Guangyu Liu, Longyu Li, Xinlin Yang, Polymers for advanced technologies . 2008,第12期

机译：制备二氧化硅/聚合物杂化微球及相应的带有官能团的空心聚合物微球
3. Facile synthesis of silica/polymer hybrid microspheres and hollow polymer microspheres [J] . Guangyu Liu, Han Zhang, Xinlin Yang Polymer: The International Journal for the Science and Technology of Polymers . 2007,第20期

机译：二氧化硅/聚合物杂化微球和空心聚合物微球的简便合成
4. Preparation of Double-shelled BaTiO_3 Composite Hollow Microspheres by Template Method [C] . Huifang Xu, Haijiao Zhang, Jianwei Song International Conference on Chemical Engineering and Advanced Materials . 2011

机译：用模板法制备双壳BATIO_3复合空心微球
5. Inorganic complexes as comonomers in the formation of porous network polymers: Investigation of the ability of highly crosslinked network polymers to isolate and stabilize reactive inorganic complexes and evidence of the template effect in metallo-network polymers. [D] . Krebs, John Franklin. 1997

机译：无机络合物作为多孔网络聚合物形成中的共聚单体：研究高度交联的网络聚合物分离和稳定反应性无机络合物的能力，以及金属网络聚合物中模板作用的证据。
6. Self-templated Synthesis of Nickel Silicate Hydroxide/Reduced Graphene Oxide Composite Hollow Microspheres as Highly Stable Supercapacitor Electrode Material [O] . Yanhua Zhang, Wenjie Zhou, Hong Yu, 2017

机译：氢硅酸镍/还原氧化石墨烯复合空心微球的自模板合成作为高稳定性超级电容器电极材料
7. Synthesis of a Au/Silica/Polymer Trilayer Composite and the Corresponding Hollow Polymer Microsphere with a Movable Au Core [O] . -1

机译：Au /二氧化硅/聚合物三层复合材料的合成和可移动Au芯的相应中空聚合物微球

Alternating Silica/Polymer Multilayer Hybrid Microspheres Templates for Double-shelled Polymer and Inorganic Hollow Microstructures

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