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Nanocrystalline Zn_(0.9)Mn_(0.1)S Thin Film: Case Studies

机译:纳米Zn_(0.9)Mn_(0.1)S薄膜的研究

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摘要

Problem statement: The high quality of ZnS:Mn nanocrystals is important in nanotechnology industries. The perfect chemical procedure is significant to produce the best of nanocrystals. Hence, this research is concern on the good chemical method in processing manganese doped zinc sulphide nanocrystals. Approach: For the first step, Mn doped ZnS nanocrystals were synthesized by using sol gel spin coating method. After the crystals were obtained, the properties of ZnS:Mn~(2+) on morphology, optical and electrical were determined by using Field Emission Scanning Electron Microscopy (FE-SEM), Ultra Violet Visible Spectroscopy (UV-Vis), Photoluminescence Spectrophotometer (PL) and current-voltage measurement (I-V). Results: The particle has diameter size around 22 nm. In this experiment it was found that the current increases with the increasing of applied voltage (-10 V to 10 V). UV-Vis spectra shows appearance of an absorption peak at 250 nm meanwhile in PL analysis spectra, the sample has been recorded at room temperature and two emissions peaks at blue and orange emissions were observed. Conclusion: Manganese doped zinc sulphide was successfully synthesized using sol gel spin coating method and it performs in good quality.
机译:问题陈述:高质量的ZnS:Mn纳米晶体在纳米技术行业中很重要。完美的化学程序对于生产最佳的纳米晶体至关重要。因此,本研究关注于加工锰掺杂的硫化锌纳米晶体的良好化学方法。方法:第一步,通过溶胶凝胶旋涂法合成了锰掺杂的ZnS纳米晶体。获得晶体后,使用场发射扫描电子显微镜(FE-SEM),紫外可见光谱(UV-Vis),光致发光分光光度计测定ZnS:Mn〜(2+)的形貌,光学和电学性质。 (PL)和电流电压测量(IV)。结果:该颗粒的直径大小约为22 nm。在该实验中,发现电流随着施加电压的增加(-10 V至10 V)而增加。 UV-Vis光谱显示在250 nm处出现一个吸收峰,而在PL分析光谱中,该样品已在室温下记录,并且观察到蓝色和橙色发射处的两个发射峰。结论:溶胶凝胶旋涂法成功地合成了锰掺杂的硫化锌,且质量良好。

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  • 来源
    《American journal of applied sciences》 |2011年第8期|p.822-825|共4页
  • 作者单位

    Department of Electrical, Electronic and Systems Engineering, Computer and Network Security Research Group, Faculty of Engineering and Built Environment, University Kebangsaan Malaysia, 43600 UKM Bangi, Selangor, Malaysia;

    Centre of Pre-University, University Malaysia Sarawak, 94300 Kota Samarahan, Sarawak, Malaysia;

    Institute of Micro Engineering and Nanoelectronic, University Kebangsaan Malaysia, 43600 UKM, Bangi, Selangor, Malaysia;

    Institute of Micro Engineering and Nanoelectronic, University Kebangsaan Malaysia, 43600 UKM, Bangi, Selangor, Malaysia;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    sol gel; spin coating; zinc sulphide; manganese; optical; electrical;

    机译:溶胶凝胶旋涂硫化锌锰;光学电的;

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