Study of metallic components of historical organ pipes using synchrotron radiation X-ray microfluorescence imaging and grazing incidence X-ray diffraction

L. K. Herrera; A. Justo; A. Mu?oz-Páez; J. A. Sans; G. Martínez-Criado

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Study of metallic components of historical organ pipes using synchrotron radiation X-ray microfluorescence imaging and grazing incidence X-ray diffraction

机译：利用同步辐射X射线微荧光成像和掠入射X射线衍射研究历史器官管的金属成分

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摘要

A comparative study of the composition and microstructure of two different brass alloys from reed pipes, one from a Spanish baroque organ and the other from a modern one, was carried out. This study allowed us to determine the procedure followed to produce the brass used to make ancient reed pipes. Moreover the distribution and correlation of lead and other trace elements present into the main component of the brass, the copper and zinc phases, of the historical tongues and shallots were established. This chemical composition was compared with that of a tongue from a twentieth-century organ. The whole study was accomplished using a combination of laboratory and synchrotron radiation techniques. X-ray fluorescence was the technique used to obtain elemental and chemical imaging of the main phases and the trace elements at a sub-micrometer scale.

机译：对芦苇管中两种不同黄铜合金的成分和微观结构进行了比较研究，一种来自西班牙巴洛克风琴，另一种来自现代烟斗。这项研究使我们能够确定生产古代芦苇管用黄铜所遵循的程序。此外，还建立了铅和其他微量元素在黄铜，铜和锌相，历史舌头和胡葱的主要成分中的分布和相关性。将该化学组成与二十世纪器官的舌头进行了比较。整个研究是通过结合实验室和同步辐射技术完成的。 X射线荧光技术是用于在亚微米级获得主要相和微量元素的元素和化学成像的技术。

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来源
《Analytical and Bioanalytical Chemistry》 |2009年第7期|1969-1975|共7页
作者
L. K. Herrera; A. Justo; A. Mu?oz-Páez; J. A. Sans; G. Martínez-Criado;
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作者单位

European Synchrotron Radiation Facility BP 220 38043 Grenoble Cedex France;

European Synchrotron Radiation Facility BP 220 38043 Grenoble Cedex France;

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原文格式 PDF
正文语种 eng
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关键词
Reed pipes; Brass alloys; Grazing incidence X-ray diffraction (GIXRD); μ-Raman spectroscopy (RS); μX-ray fluorescence (μXRF); Synchrotron radiation;

机译：簧片管;黄铜合金;掠入射X射线衍射（GIXRD）;μ拉曼光谱（RS）;μX射线荧光（μXRF）;同步辐射;

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专利

1. Study of metallic components of historical organ pipes using synchrotron radiation X-ray microfluorescence imaging and grazing incidence X-ray diffraction [J] . Herrera L.K., Justo A., Mu?oz-Páez A., Analytical and bioanalytical chemistry . 2009,第7期

机译：利用同步辐射X射线微荧光成像和掠入射X射线衍射研究历史器官管的金属成分
2. A Combined Voltammetric and Synchrotron Radiation-Grazing Incidence X-ray Diffraction Study of the Electrocrystallization of Zinc Tetracyanoquinodimethane [J] . Jean-Pierre Veder, Ayman Nafady, Graeme Clarke Australian Journal of Chemistry: A Journal for the Publication of Original Research in All Branches of Chemistry . 2012,第3期

机译：伏安法和同步辐射辐射-放牧相结合的X射线衍射研究四氯化锌对氨基喹啉锌的电结晶
3. An in situ electrochemical impedance spectroscopy/synchrotron radiation grazing incidence X-ray diffraction study of the influence of acetate on the carbon dioxide corrosion of mild steel [J] . Roland De Marco, Zhong-Tao Jiang, Doug John, Electrochimica Acta . 2007,第11期

机译：醋酸盐对低碳钢二氧化碳腐蚀影响的原位电化学阻抗谱/同步辐射放牧入射X射线衍射研究
4. Structure of the 3C-SiC(100) 5×2 Surface Reconstruction Investigated by Synchrotron Radiation Based Grazing Incidence X-ray Diffraction [C] . M. Silly, H. Enriquez, J. Roy, European Conference on Silicon Carbide and Related Materials . 2007

机译：由基于同步辐射的放射入射X射线衍射研究的3C-SiC（100）5×2表面重建的结构
5. Crystal chemistry of open framework sulfides and x-ray diffraction study with synchrotron radiation/imaging plate system. [D] . Tan, Kemin. 1996

机译：开放式框架硫化物的晶体化学和同步辐射/成像板系统的X射线衍射研究。
6. Urease and hexadecylamine-urease films at the air-water interface: an x-ray reflection and grazing incidence x-ray diffraction study. [O] . D Gidalevitz, Z Huang, S A Rice 1999

机译：空气-水界面处的脲酶和十六烷基脲脲酶薄膜：X射线反射和掠入射X射线衍射研究。
7. Small-Angle X-Ray Scattering (SAXS), Ultra-Small Angle X-Ray Scattering (USAXS), Fluctuation X-Ray Scattering (FXS), Wide-Angle X-Ray Scattering (WAXS), Grazing-Incidence Small-Angle X-Ray Scattering (GISAXS), Grazing-Incidence Wide-Angle X-Ray Scattering (GIWAXS), Small-Angle Neutron Scattering (SANS), Grazing-Incidence Small-Angle Neutron Scattering (GISANS), X-Ray Diffraction (XRD), Powder X-Ray Diffraction (PXRD), Wide-Angle X-Ray Diffraction (WAXD), Grazing- Incidence X-Ray Diffraction (GIXD) and Energy-Dispersive X-Ray Diffraction (EDXRD) Comparative Study on Malignant and Benign Human Cancer Cells and Tissues under Synchrotron Radiation [O] . Alireza Heidari 2017

机译：小角X射线散射（萨克斯），超小角X射线散射（USAX），波动X射线散射（FXS），广角X射线散射（蜡），放牧发生小角度x - 射线散射（吉即），放牧入射广角X射线散射（Giwaxs），小角度中子散射（SAN），放牧发生小角度中子散射（Gisans），X射线衍射（XRD），粉末X射线衍射（PXRD），广角X射线衍射（WAXD），放牧发病X射线衍射（GIXD）和能量分散X射线衍射（EDXRD）对恶性和良性人体癌细胞的比较研究和同步辐射下的组织
8. Grazing Incidence X-Ray Scattering Study of Defect Structures in MBE GaAs/Si Using Synchrotron Radiation [R] . Laderman, S. S. , Kortright, J. , Scott, M. , 1987

机译：基于同步辐射的mBE Gaas / si缺陷结构的放大入射X射线散射研究

Study of metallic components of historical organ pipes using synchrotron radiation X-ray microfluorescence imaging and grazing incidence X-ray diffraction

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