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Neutron diffraction characterization of Japanese artworks of Tokugawa age

机译:德川时代日本艺术品的中子衍射表征

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Neutron time-of-flight diffraction technique has been used to characterize some Japanese historical artifacts. With this method, metal samples can be analyzed in their bulk properties without need of sampling. Results shown here were obtained at the Italian Neutron Experimental Station (INES@ISIS) located at the pulsed neutron source ISIS (UK). The parallel use of a scanning electron microscope equipped with an energy-dispersive X-ray fluorescence device (SEM-EDX) permitted a full quantitative characterization of the investigated samples, namely four hand-guards (Tsubas) of Japanese swords attributed to the Tokugawa age. In particular, we were able to obtain, in a totally non-invasive non-destructive way, a full quantitative phase characterization of the samples, a detailed Bragg peak broadening analysis, and a quantitative texture determination. These results, complemented with those obtained via the traditional analysis method of SEM-EDX, allowed a full characterization of both the bulk and the surface of the artifacts.
机译:中子飞行时间衍射技术已被用来表征一些日本历史文物。使用这种方法,无需取样即可分析其金属性质。此处显示的结果是从位于脉冲中子源ISIS(UK)的意大利中子实验站(INES @ ISIS)获得的。并行使用配有能量色散X射线荧光装置(SEM-EDX)的扫描电子显微镜,可以对所研究的样品进行全面的定量表征,即属于德川时代的日本剑的四个护手(Tsubas)。 。尤其是,我们能够以完全非侵入性的非破坏性方式获得样品的完整定量相特征,详细的布拉格峰加宽分析和定量纹理测定。这些结果与通过SEM-EDX的传统分析方法获得的结果相辅相成,可以完全表征工件的体积和表面。

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