Electrodeposited non-stoichiometric tungstic acid for electrochromic applications: film growth modes, crystal structure, redox behavior and stability

Pugolovkin Leonid V.; Cherstiouk Olga V.; Plyasova Lyudmila M.; Molina Irina Yu.; Kardash Tatyana Yu.; Stonkus Olga A.; Yatsenko Dmitriy A.; Kaichev Vasily V.; Tsirlina Galina A.

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Electrodeposited non-stoichiometric tungstic acid for electrochromic applications: film growth modes, crystal structure, redox behavior and stability

机译：用于电致变色应用的电沉积非化学计量钨酸：薄膜生长模式，晶体结构，氧化还原行为和稳定性

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摘要

Bath composition for cathodic electrodeposition of non-stoichiometric hydrated tungstic acid with high electrochromic efficiency is optimized with account for selective electroreduction of certain isopolytungstates. XRD data for thin electrodeposited films and chemically synthesized bulk tungstic acid dihydrate are compared in the context of reversible oxidation and reduction in hydrogen atmosphere, in presence of Pt catalyst. XPS and TEM techniques are attracted to understand the nature of reversible and less reversible transformations of films in the course of their storage and operation. (C) 2016 Elsevier B.V. All rights reserved.

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来源
《Applied Surface Science》 |2016年第ptab期|786-793|共8页
作者
Pugolovkin Leonid V.; Cherstiouk Olga V.; Plyasova Lyudmila M.; Molina Irina Yu.; Kardash Tatyana Yu.; Stonkus Olga A.; Yatsenko Dmitriy A.; Kaichev Vasily V.; Tsirlina Galina A.;
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作者单位

Moscow MV Lomonosov State Univ, Dept Electrochem, Moscow, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia|Novosibirsk State Univ, Novosibirsk, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia|Novosibirsk State Univ, Novosibirsk, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia|Novosibirsk State Univ, Novosibirsk, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia|Novosibirsk State Univ, Novosibirsk, Russia;

SB RAS, Boreskov Inst Catalysis, Novosibirsk, Russia|Novosibirsk State Univ, Novosibirsk, Russia;

Moscow MV Lomonosov State Univ, Dept Electrochem, Moscow, Russia;

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正文语种 eng
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关键词
Oxide electrodeposition; Electrochromic films; Tungstic acid; Non-stoichiometry;

机译：氧化物电沉积;电致变色膜;钨酸;非化学计量;

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1. Preparation, characterisation and electrochromic property of mesostructured tungsten oxide films via a surfactant templated sol-gel process from tungstic acid [J] . Wei Wang, Yongxin Pang, Simon N. B. Hodgson Journal of Sol-Gel Science and Technology . 2010,第1期

机译：钨酸通过表面活性剂模板溶胶凝胶法制备介孔氧化钨薄膜，表征及电致变色性能
2. Preparation, characterisation and electrochromic property of mesostructured tungsten oxide films via a surfactant templated sol–gel process from tungstic acid [J] . Wei Wang, Yongxin Pang, Simon N. B. Hodgson Journal of Sol-Gel Science and Technology . 2010,第1期

机译：钨酸通过表面活性剂模板溶胶-凝胶法制备介孔氧化钨薄膜，表征和电致变色性能
3. Colloidal tungstic oxide films for electrochromic applications: Preliminary studies [J] . P K Varshney, Nidhi, R Ramachandran, Indian Journal of Pure & Applied Physics . 1999,第4期

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4. Characterization of electrodeposited nano-Structured cerium-based mixed oxide films for electrochromic device [C] . T.Yoshino, J.Nagai, H.Masuda The Meeting of the Electrochemical Society . 2003

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5. The optical properties of lithium tungsten bronze single crystals and thin films for electrochromic window device applications. [D] . Berera, Geetha Poonacha. 1992

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6. Early-Stage Growth Mechanism and Synthesis Conditions-Dependent Morphology of Nanocrystalline Bi Films Electrodeposited from Perchlorate Electrolyte [O] . Daria Tishkevich, Sergey Grabchikov, Tatiana Zubar, 2020

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7. Preparation, characterisation and electrochromic property of mesostructured tungsten oxide films via a surfactant templated sol–gel process from tungstic acid [O] . Wang, W. (Wei), Pang, Y. X. (Yongxin), Hodgson, S. N. B. (Simon) 2010

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Electrodeposited non-stoichiometric tungstic acid for electrochromic applications: film growth modes, crystal structure, redox behavior and stability

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