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首页> 外文期刊>Applied Surface Science >Electrodeposition of NiPd alloy from aqueous chloride electrolytes
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Electrodeposition of NiPd alloy from aqueous chloride electrolytes

机译：用氯化物水溶液电沉积NiPd合金

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摘要

Presented results describing properties of alloys deposited at potentiostatic conditions in Ni2+ - Pd2+ - Cl- - H2O system. Electrolysis parameters were defined based on results of thermodynamic analysis as well as voltammetry coupled with electrochemical quartz crystal microbalance (EQCM). Influence of electrode potential and electrolyte components concentration on alloy composition, morphology and its structure was investigated. Alloys were deposited at different Ni(II) and Pd(II) complexes concentrations. Results indicated possibilities of electrochemical synthesis of alloys of wide composition range. Deposits structure as well as crystallites size were discussed based on results of XRD measurements. Alloys composition was determined with the use of energy dispersive spectroscopy (EDS). Morphology of alloys was characterized with the use of scanning electron microscopy (SEM). (C) 2016 Elsevier B.V. All rights reserved.
机译：呈现的结果描述了在恒电位条件下在Ni2 +-Pd2 +-Cl--H2O体系中沉积的合金的性能。根据热力学分析以及伏安法和电化学石英晶体微量天平（EQCM）的结果定义了电解参数。研究了电极电位和电解质组分浓度对合金成分，形貌及其结构的影响。合金以不同的Ni（II）和Pd（II）配合物浓度沉积。结果表明了广泛合成范围合金的电化学合成的可能性。根据XRD测量结果讨论了沉积物的结构以及微晶的尺寸。使用能量色散光谱法（EDS）确定合金成分。合金的形貌通过扫描电子显微镜（SEM）表征。 （C）2016 Elsevier B.V.保留所有权利。

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  • 来源
    《Applied Surface Science》 |2016年第ptab期|809-816|共8页
  • 作者

    Mech K.; Wrobel M.; Wojnicki M.; Mech-Piskorz J.; Zabinski P.; Kowalik R.;

  • 作者单位

    AGH Univ Sci & Technol, Acad Ctr Mat & Nanotechnol, Al A Mickiewicza 30, PL-30059 Krakow, Poland;

    AGH Univ Sci & Technol, Fac Met Engn & Ind Comp Sci, Al A Mickiewicza 30, Krakow, Poland;

    AGH Univ Sci & Technol, Fac Non Ferrous Met, Dept Phys Chem & Met Non Ferrous Met, Al A Mickiewicza 30, PL-30059 Krakow, Poland;

    Polish Acad Sci, Inst Phys Chem, Ul Kasprzaka 44-52, PL-01224 Warsaw, Poland;

    AGH Univ Sci & Technol, Fac Non Ferrous Met, Dept Phys Chem & Met Non Ferrous Met, Al A Mickiewicza 30, PL-30059 Krakow, Poland;

    AGH Univ Sci & Technol, Fac Non Ferrous Met, Dept Phys Chem & Met Non Ferrous Met, Al A Mickiewicza 30, PL-30059 Krakow, Poland;

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  • 正文语种 eng
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  • 关键词

    Ni-Pd alloy; Electrodeposition; Voltammetry; Chloride electrolytes;

    机译：Ni-Pd合金;电沉积;伏安法;氯化物电解质;

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