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Effects of carbon fiber surface characteristics on interfacial bonding of epoxy resin composite subjected to hygrothermal treatments

机译:碳纤维表面特性对湿热处理环氧树脂复合材料界面结合的影响

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摘要

The changes of interfacial bonding of three types of carbon fibers/epoxy resin composite as well as their corresponding desized carbon fiber composites subjecting to hygrothermal conditions were investigated by means of single fiber fragmentation test. The interfacial fracture energy was obtained to evaluate the interfacial bonding before and after boiling water aging. The surface characteristics of the studied carbon fiber were characterized using X-ray photoelectron spectroscopy. The effects of activated carbon atoms and silicon element at carbon fiber surface on the interfacial hygrothermal resistance were further discussed. The results show that the three carbon fiber composites with the same resin matrix possess different hygrothermal resistances of interface and the interfacial fracture energy after water aging can not recovery to the level of raw dry sample (irreversible changes) for the carbon fiber composites containing silicon. Furthermore, the activated carbon atoms have little impact on the interfacial hygrothermal resistance. The irreversible variations of interfacial bonding and the differences among different carbon fiber composites are attributed to the silicon element on the carbon fiber bodies, which might result in hydrolyzation in boiling water treatment and degrade interfacial hygrothermal resistance.
机译:通过单纤维断裂试验研究了三种类型的碳纤维/环氧树脂复合材料及其相应的变尺寸碳纤维复合材料在湿热条件下的界面粘结变化。获得界面断裂能以评估沸水老化前后的界面结合。使用X射线光电子能谱表征了研究碳纤维的表面特性。进一步讨论了碳纤维表面活性炭原子和硅元素对界面耐湿热性的影响。结果表明,三种具有相同树脂基体的碳纤维复合材料具有不同的界面耐湿热性,水老化后的界面断裂能不能恢复到含硅碳纤维复合材料的原始干样品水平(不可逆变化)。此外,活性炭原子对界面耐湿热性几乎没有影响。界面键的不可逆变化以及不同碳纤维复合材料之间的差异归因于碳纤维体上的硅元素,这可能导致沸水处理中发生水解并降低界面耐湿热性。

著录项

  • 来源
    《Applied Surface Science》 |2014年第1期|666-672|共7页
  • 作者单位

    Key Laboratory of Aerospace Advanced Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing 100191, China;

    Key Laboratory of Aerospace Advanced Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing 100191, China;

    Key Laboratory of Aerospace Advanced Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing 100191, China;

    Key Laboratory of Aerospace Advanced Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing 100191, China;

    Key Laboratory of Aerospace Advanced Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing 100191, China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Carbon fiber; Composites; Hygrothermal treatment; Single fiber fragmentation test; Interfacial bonding;

    机译:碳纤维;复合材料;湿热处理;单纤维破碎测试;界面结合;

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