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Growth Dynamics And Thermal Stability Of Ni Nanocrystalline Nanowires

机译:Ni纳米晶纳米线的生长动力学和热稳定性

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摘要

The growth dynamics and the thermal stability of a Ni nanocrystalline nanowire (NNW) model system fabricated using electrochemical deposition has been investigated using X-ray diffraction, scanning and transition electron microcopy, and differential scanning calorimetry (DSC). It has been found that the thermal stability of the Ni-NNW is dominated by the microstructure movement and the grain boundary rotation mechanism at temperature ranging from 400 to 600 °C. The Ni-NNW experiences the Rayleigh instability at temperature approaching the melting point. The observed fragment separation in the Rayleigh phase-transition is much greater than that expected theoretically.
机译:使用X射线衍射,扫描和过渡电子显微镜以及差示扫描量热法(DSC)研究了使用电化学沉积方法制备的Ni纳米晶纳米线(NNW)模型系统的生长动力学和热稳定性。已经发现,Ni-NNW的热稳定性在400至600℃范围内的温度下由显微组织运动和晶界旋转机制决定。 Ni-NNW在接近熔点的温度下经历瑞利不稳定性。在瑞利相变中观察到的碎片分离远大于理论上的预期。

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  • 来源
    《Applied Surface Science》 |2011年第23期|p.9991-9995|共5页
  • 作者单位

    Faculty of Materials, Optoelectronics and Physics, Xiangtan University, Xiangtan, Hunan, 411105, China Key Laboratory of Low Dimensional Materials and Application Technology, Xiangtan University, Ministry of Education, Xiangtan, Hunan 411105, China;

    Faculty of Materials, Optoelectronics and Physics, Xiangtan University, Xiangtan, Hunan, 411105, China Key Laboratory of Low Dimensional Materials and Application Technology, Xiangtan University, Ministry of Education, Xiangtan, Hunan 411105, China;

    Faculty of Materials, Optoelectronics and Physics, Xiangtan University, Xiangtan, Hunan, 411105, China Key Laboratory of Low Dimensional Materials and Application Technology, Xiangtan University, Ministry of Education, Xiangtan, Hunan 411105, China;

    National Physical Laboratory (NPL), Analytical Science Division, Hampton road, Teddington, Middlesex, 7W7 I OLW, UK;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Nanocrystalline materials; Grain boundaries; Thermal properties; Rayleigh instability;

    机译:纳米晶材料;晶界;热性能;瑞利不稳定性;

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