Annealing Improves Tribological Property Of Poly(Octadecene-Alt-Maleic Anhydride) Self-Assembled Film

ShiyongSong; Lei Liu; JunyanZhang

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Annealing Improves Tribological Property Of Poly(Octadecene-Alt-Maleic Anhydride) Self-Assembled Film

机译：退火改善了聚（十八碳烯-ALT-马来酸酐）自组装膜的摩擦学性能

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A poly(octadecene-alt-maleic anhydride) (POMA) film was covalently immobilized on N-[3-(trimethoxylsilyl)propyl]ethylenediamine self-assembled monolayer modified silicon surface. Attenuated total reflectance Fourier transform infrared spectra were used to confirm the chemical bonding. Water contact angles and ellipsometric thicknesses were measured before and after annealing treatment. Atomic force microscopy was applied for top morphology, surface adhesion force and friction force. Anti-wear properties of the films were also evaluated on a ball-on-plate tribometer. It was found that annealing treatment which would evoke a conformation transform thermodynamically, was a critical step in the preparation of anti-wear films, especially for polymer ones. The correlation between structure and tribological property was revealed, which has profound meaning in designing excellent anti-wear nano-coatings used in microelectronic mechanical systems (MEMS).

机译：聚（十八碳烯-马来酸酐）（POMA）膜共价固定在N- [3-（三甲氧基甲硅烷基）丙基]乙二胺自组装单层改性硅表面上。使用衰减的全反射傅立叶变换红外光谱确认化学键合。在退火处理之前和之后，测量水接触角和椭偏厚度。原子力显微镜用于顶部形态，表面粘附力和摩擦力。膜的抗磨性能也用球上摩擦计评估。已经发现，退火处理会引起构象在热力学上发生转变，是制备抗磨膜，特别是对于聚合物膜的关键步骤。揭示了结构与摩擦学性质之间的相关性，这对于设计用于微电子机械系统（MEMS）的优异抗磨纳米涂层具有深远的意义。

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《Applied Surface Science》 |2011年第23期|p.10254-10260|共7页
作者
ShiyongSong; Lei Liu; JunyanZhang;
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作者单位

Pharmaceutic College ofHenan University, Kaifeng 475004, China;

Pharmaceutic College ofHenan University, Kaifeng 475004, China;

Pharmaceutic College ofHenan University, Kaifeng 475004, China State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China;

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正文语种 eng
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关键词
POMA; Self-assembled film; Friction; Anti-wear, AFM;

机译：POMA;自组装薄膜;摩擦;抗磨;AFM;

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1. Modification of poly(octadecene-alt-maleic anhydride) films by reaction with functional amines [J] . Schmidt U., Zschoche S., Werner C. Journal of Applied Polymer Science . 2003,第8期

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3. Stable Self-Assembled Multilayer Films of Diazo Resin and Poly(maleic anhydride-co-styrene) Based on Charge-Transfer Interaction [J] . Yongjun Zhang, Weixiao Cao Langmuir: The ACS Journal of Surfaces and Colloids . 2001,第16期

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Annealing Improves Tribological Property Of Poly(Octadecene-Alt-Maleic Anhydride) Self-Assembled Film

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