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Electrophoreted Zn-tio_2-zno Nanocomposite Coating Films For Photocatalytic Degradation Of 2-chlorophenol

机译:电泳Zn-tio_2-zno纳米复合涂膜对2-氯苯酚的光催化降解

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摘要

TiO_2-ZnO nano-powders with different TiO_2/ZnO ratios have been synthesized by hydrothermal method. Nanocomposite coating films consisting of TiO_2-ZnO and Zn with thickness of 20 μm have been electrophoreted on steel plates by rapid plating from a ZnO-based alkaline bath. X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis were used to investigate the structure, the size distribution, and the composition of prepared nano-powders and plated materials. The effect of the operating parameters such as powder contents, pH and current density on the electrophoresis process has been investigated and optimum conditions of coating process were determined. Corrosion properties of plated samples have been studied by salt spray test. The catalytic activity of the prepared nanocomposite Zn-TiO_2-ZnO films for the photocatalytic degradation of 2-chlorophenol (2-CP) was measured.
机译:采用水热法合成了不同TiO_2 / ZnO比的TiO_2-ZnO纳米粉。通过从基于ZnO的碱性浴中快速电镀,在钢板上电泳了由TiO_2-ZnO和Zn组成的纳米复合涂层膜,其厚度为20μm。用X射线衍射,扫描电子显微镜和能量色散X射线分析法研究了制备的纳米粉体和镀层材料的结构,尺寸分布和组成。研究了诸如粉末含量,pH和电流密度等操作参数对电泳过程的影响,并确定了最佳的涂布工艺条件。通过盐雾试验研究了镀层样品的腐蚀性能。测量了制备的纳米复合Zn-TiO_2-ZnO薄膜对2-氯苯酚(2-CP)的光催化降解的催化活性。

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