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Dissolution Of Synthetic And Bovine Bone-derived Hydroxyapatites Fabricated By Hot-pressing

机译:热压法制备的合成和牛骨羟基磷灰石的溶解

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Dissolving behavior of hydroxyapatite (HA) ceramics prepared from bovine bone (BHA) was investigated and compared with synthetic HA. BHA power was obtained by calcining at 800℃ for 1 h to remove organics and then attritor-milling for 24 h. Synthetic HA and BHA powders were prepared by hot-pressing at 1000℃ for 0.5 h under the pressure of 30 MPa in Ar atmosphere. Sintered densities of the synthetic HA and the BHA were about 96% and 95%, respectively. The BHA consisted of mainly HA and small amount of magnesium oxide. Immersion test revealed that there was no clear evidence of dissolution for the BHA, whereas extensive dissolution on the surface of the synthetic HA occurred in buffered water. Accordingly, dense hydroxyapatite from bovine bone was more stable than synthetic HA in liquid environment.
机译:研究了由牛骨(BHA)制成的羟基磷灰石(HA)陶瓷的溶解行为,并将其与合成HA进行了比较。通过在800℃下煅烧1小时以去除有机物,然后进行粉碎机研磨24小时,可获得BHA功率。在Ar气氛中,在30 MPa的压力下,于1000℃热压0.5 h,制得合成的HA和BHA粉末。合成HA和BHA的烧结密度分别为约96%和95%。 BHA主要由HA和少量氧化镁组成。浸入测试表明,没有明确证据表明BHA溶解,而合成HA的表面在缓冲水中发生了广泛溶解。因此,在液体环境中,来自牛骨的致密羟基磷灰石比合成HA更稳定。

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